The chemical composition of oregano essential oil of different origin extracted from oregano plants grown in south-eastern Poland was analysed using the gas chromatography mass spectrometry (GC-MS) and gas chromatography flame ionization detector (GC-FID). The dominant compound was sabinene; its percentage proportion ranged from 10.85% to 25.46%, depending on the ecotype studied. Moreover, the ...

Simple, cheap and green protocol for effective conversion of alcohols to corresponding carbonyl compounds in the presence of H14[NaP5W30O110] and ammonium nitrate is reported. The products were characterized by FT-IR and comparison of their physical properties with those reported in the literatures. The progress of the reaction was monitored by thin layer chromatography (TLC) technique. The ali...

Accurate methods are described for the qualitative and quantitative determination of medazepam, diazepam, and nitrazepam in 5 ml of whole blood. Medazepam and diazepam are analyzed intact and nitrazepam is chromatographed as its trimethylsilyl derivative by flame-ionization gas-chromatography on “1% OV-17.” A supplementary column of “2% OV-1” is used to separate nitrazepam TMS from diazepam whe...

Adsorbent tube samples are collected by drawing workplace air through either coconut shell charcoal or Anasorb 747 tubes with personal sampling pumps. Diffusive samples are collected by exposing either 3M 3520 Organic Vapor Monitors (OVMs) or SKC 575-002 Passive Samplers to workplace air. Samples are desorbed with 60/40 (v/v) N,N-dimethylformamide/carbon disulfide (DMF/CS2) and analyzed by gas ...

Vacuum-outlet operation of short fused-silica open tubular columns for gas chromatography provides benefits to analysis speed by increasing the optimum velocity while minimizing the loss in resolution. Vacuum-outlet operation of a column with a gas chromatographic detector necessitates that the detector also be under vacuum. Simple modifications were made to a gas chromatograph]flame Ž . ioniza...

simple, cheap and green protocol for effective conversion of alcohols to corresponding carbonyl compounds in the presence of h14[nap5w30o110] and ammonium nitrate is reported. the products were characterized by ft-ir and comparison of their physical properties with those reported in the literatures. the progress of the reaction was monitored by thin layer chromatography (tlc) technique. the ali...

This paper describes a new method for qualitative and quantitative assay of abscisic acid and other acidic plant hormones, such as indoleacetic acid and the gibberellins, by the gas-liquid chromatography of their trimethylsilyl derivatives. Interfering substances in plant extracts were largely removed by preliminary column chromatography with carbon-celite and elution of the abscisic acid with ...

Hyphenated gas chromatography (GC) (Chaturvedi & Nanda, 2010; Coleman III & Gordon, 2006) mainly refers to the coupling of the high-performance separation technique of gas chromatography with 1) information-rich and sophisticated GC detectors which otherwise can be mostly operated as a stand-alone instrument for chemical analysis, and 2) automated online sample preparation systems. The term “hy...

A bstract. This paper describes a new method for qualitative and quantitative assay of abscisic acid and other acidic plant hormones, such as indoleacetic acid and the gibberellins, by the gas-liquid chromatography of their trimethylsilyl derivatives. Interfering substances in plant extracts were largely removed by preliminary oolumn chromatography with carbon-celite and elution of the absoisic...

background: nanotechnology is a new approach that has been lionized in recent years. one of its applications is its consumption as an absorbent. in this study, the single-wall carbon nanotubes (swcnts) were used as an absorbent for sampling benzene in the air. materials and methods: for this study, swcnts manufactured by iran and skc’s activated charcoal were used for sampling benzene vapors. p...