the perovskite-type oxides strontium-substituted lanthanum nickelate (lsno) were prepared by a coprecipitation method in the present of octanoic acid as surfactant. the phase composition, morphology,lattice parameters and size of nanoparticles in these materials were characterized through fourier transform infrared spectroscopy (ft-ir), x-ray diffraction (xrd), scanning electron microscopy (sem...

zro2 nanopowder was prepared by the sol-gel auto-combustion method. the product was characterized by x-ray diffraction (xrd), energy dispersive analysis of x-ray (edx) and scanning electron microscopy (sem). the average crystalline size of zro2 was obtained 62 nm. also, photocatalytic removal of nitrophenol from aqueous solution by using nanoscale zro2 under uv light irradiation was studied. th...

Laser-induced breakdown spectroscopy (LIBS) is applied to characterize the formation of porous hydroxyapatite layers on the surface of 0.8CaSiO₃-0.2Ca₃(PO₄)₂ biocompatible eutectic glass immersed in simulated body fluid (SBF). Compositional and structural characterization analyses were also conducted by field emission scanning electron microscopy (FESEM), energy dispersive X-ray spectroscopy (E...

For most materials science oriented applications incoherent cathodoluminescence (CL) is of main interest, for which the recombination electron–hole pairs yields emission light. However, signal superimposed by coherently excited photons, similar to situation X-rays in Energy-Dispersive X-ray spectra (EDX). In EDX two very different processes superimpose each spectrum: Bremsstrahlung and characte...

This work examines the use of new hydrophobic ionic liquid derivatives, namely octadecylammonium tosylate (ODA-TS) and oleylammonium tosylate (OA-TS) for corrosion protection of steel in 1 M hydrochloric acid solution. Their chemical structures were determined from NMR analyses. The surface activity characteristics of the prepared ODA-TS and OA-TS were evaluated from conductance, surface tensio...

Rapidly developing field of nanobiotechnology dealing with metallic nanoparticle (MNP) synthesis is primarily lacking control over size, shape, dispersity, yield, and reaction time. Present work describes an ecofriendly method for the synthesis of silver nanoparticles (AgNPs) by cell free extract (CFE) of Saccharomyces boulardii. Parameters such as culture age (stationary phase growth), cell ma...

co-fe films were electrodeposited on cu substrate from electrolytes with different co concentration  levels. x-ray diffraction (xrd) was used  to  investigate  the  films  crystal  structures. the  results  indicate that  if  the  co  concentration  is  less  that  the  fe  concentration,  the cubic  structure  appears  in  the  films, while  the  hexagonal  structure dominates when  the co  co...

limn2o4 spinel cathode materials have been successfully synthesized by solid-state reaction. surface of these particles were modified by nanostructured lifepo4 via sol gel dip coating method. synthesized products were characterized by thermally analyzed by thermogravimetric and differential thermal analysis(tg/dta), x-ray diffraction (xrd), scanning electron microscopy (sem), and energy dispers...

A new approach is described for the recovery of precious metals (PMs: Au, Pd and Ag) with >99% efficiency from aqueous solution utilising biogas produced during the aerobic growth of Klebsiella pneumoniae. Gold was recovered from electronic scrap leachate ( approximately 95%) by this method, with some selectivity against Cu. The recovered PM solids all contained metal and sulphur as determined ...