نتایج جستجو برای: crystal structure
تعداد نتایج: 1647502 فیلتر نتایج به سال:
The SDS, PEG and CTAB roofed MgO nano powders were synthesized by co-precipitation method. The sintered nano powders was shown Fm-3m space group with cubic phase obtained by the XRD pattern. The lattice strain was calculated to be used Williamson-Hall equations (W-H). The formation of Mg-O bond and hydroxyl radicals on the surface were confirmed by the FTIR analyses. The TEM revealed that the ...
zinc oxide (zno) nanopowders were synthesized by the sol–gel method from an ethanol solution of zinc sulfate heptahydrate in the presence of diethylene glycol surfactant. detailed structural and microstructural investigations were carried out using x-ray diffraction (xrd), high-resolution transmission electron microscopy (hrtem), field emission scanning electron microscopy (fe-sem), fourier tra...
the purpose of this paper is the generalization of structure factor for rods by polygon section in two dimensional phononic crystals. if we use the plane wave expansion method (pwe) for the propagation of acoustic waves in 2d phononic crystals, structure factor will be an important quantity. in order to confirm the obtained relations, we have calculated the band structure for xy and z vibration...
the zinc(ii) complex [zn2(dmdtc)2(μ-dmdtc)2] has been synthesized directly from thiram ligand, containing a disulfide bond {dmdtc = n,n-dimethyldithiocarbamate; thiram = n,n-tetramethylthiuram disulfide}, and characterized by elemental analysis and spectroscopic methods. surprisingly thiram, undergoes a reductive disulfide bond scission upon reaction with zn2+ in methanolic media to give the [z...
The Dinuclear Cu (II) complex [{CuCl}2(μ – tppz)](PF6)2, where tppz represents tetra-2-pyridinylpyrazine, has been prepared and characterized by elemental analysis, 1H-NMR, IR and UV-vis spectroscopies. A crystal structure of the complex showed the Cu (II) are surrounded by three N atoms of tppz bridging ligand and one Cl atom. Crystal structure data are as follows: crystal system monoclinic, s...
Nanostructured Ni2As2O7 semiconductor samples were synthesized by a solid state method among As2O3 and Ni(NO3)2.6H2O raw materials at 650 °C (S1) and 750 °C (S2) as reaction temperatures. The synthesized nanomaterials were characterized by powder X-ray diffraction (PXRD) technique and F...
the effect of alkyl substituents on the c-phenyl and/or the n-phenyl ring of benzophenylhydroxamic acid on their molecular structure and hydrogen bonding has been investigated. the predominant configuration in chcl3 is determined by steric and electronic effects. substituents on the c-phenyl ring favor the cis configuration, while substituents in the n-phenyl ring favor a trans configuration. t...
وجود بیش از دو فاز مغناطیسی بویژه انتقال فاز ناپایدار فرومغناطیسی در دمای بالا ( حدود دمای اتاق ) در ترکیب بین فلزیgd2al این سوال را مطرح می سازد که آیا انتقال فاز ناشی از ناخالصی است . از آنجایی که طیف اشعه ایکس قبل و بعد از عملیات حرارتی نمونه ساختار شبکه ای ترکیب فوق را اورترومبیک نشان داده است ، طیف اشعه ایکس برای ترکیباتی با انتقال فاز مغناطیس پایدار که احتمالا ناشی از پدیده spin lat...
The co-crystal compound of 4,4'-bipyridine 3-nithrophthalic acid (1) was obtained by the reaction of 4,4'-bipyridine, 3-nithrophthalic acid and calcium chloride (1:1:1 molar ratio) in solvents mixture H2O/MeOH under solution condition. The crystal structure of this compound was determined by elemental analysis, IR spectroscopy and single crystal X-ray diffraction method. Crystallographic data f...
9-aminoacridinum acridine-9-carboxylate (1) as a proton transfer ion pair was obtained by the reaction of 9-aminoacridine, acridine-9-carboxylic acid and zinc nitrate (1:1:1 molar ratio) in solvents mixture H2O/MeOH under reflux condition. The crystal structure of this compound was determined by elemental analysis, IR spectroscopy and single crystal X-ray diffraction method. Crystallographic da...
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