An automated method has been developed to characterize the type and spatial distribution of twinning in crystal orientation maps from synchrotron X-ray Laue microdiffraction results. The method relies on a look-up table approach. Taking into account the twin axis and twin plane for plausible rotation and reflection twins, respectively, and the point group symmetry operations for a specific crys...

The crystal lattice of single-crystal silicon gives rise to anisotropic elasticity. The stiffness and compliance coefficient matrix depend on crystal orientation and, consequently, Young's modulus, the shear modulus and Poisson's ratio as well. Computer codes (in Matlab and Python) have been developed to calculate these anisotropic elasticity parameters for a silicon crystal in any orientation....

We show that the crystal orientation in polymer nanotubes and nanorods inside porous templates is controlled by the kinetics of nucleation and growth under 2D confinement. Two clear limiting cases are identified: In separated nanostructures, any crystal orientation allowing the growth of lamellar crystals along the pores appears statistically. If a bulklike surface film connects the nanostructu...

In this study, the relationship between skin structure and shear strength distribution of thin-wall injection molded polypropylene (PP) molded at different molecular weight and molecular distribution was investigated. Skin-core structure, cross-sectional morphology, crystallinity, crystal orientation, crystal morphology and molecular orientation were evaluated by using polarized optical microsc...

The synthesis and structure of (C4H3S)TeCH2CH2OC6H5 (1) (C4H3S = thiophen-2-yl) are reported and compared to those of the analogous selenium compound (C4H3S)SeCH2CH2OC6H5 previously synthesized by our group. The compound was characterized by 1H, 13C{1H}-, and 125TeNMR spectroscopy as well as by X-ray single crystal crystallography. 1 crystallizes in the monoclinic crystal system, space group P2...

manufactured single crystal components using ni-base super alloys are routinely used in the hotsections of aero engines and industrial gas turbines due to their outstanding high temperaturestrength, toughness and resistance to degradation in corrosive and oxidative environments. tocontrol the quality of the single crystal turbine blades, particular attention has been paid to grainselection, whi...

The first measurements of thermally induced depolarization in a [110] oriented cubic crystal at powerful heat release were made. It was demonstrated that depolarization in a crystal with such orientation may be less than in analogous crystals having orientation [001] or [111]. In a TGG crystal, for example, maximum depolarization value was 10% and dropped down to 3% with a further increase of r...

Three-dimensional (3D) structure of a new form of diferric mare lactoferrin has been determined at 3.8 A resolution. The protein was crystallized in a space group P2(1)2(1)2(1) with a = 80.1 A, b = 103.7 A, c = 112.2 A with a solvent content of 57%. The structure was solved by molecular replacement method using the model of native mare lactoferrin. The structure has been refined using X-PLOR to...

In the title compound, C12H15N3O2S, the 1,3-benzdioxole fragment is nearly planar [the maximum deviation being 0.0515 (14) Å], the N-N-C(=S)-N fragment is also nearly planar [the maximum deviation being 0.0480 (10) Å], and the dihedral angle between their mean planes is 23.49 (10)°. In the crystal, mol-ecules are linked by pairs of N-H⋯S hydrogen bonds, forming inversion dimers. The dimers are ...

The effects of horizontal high magnetic field (8 T) on both the orientation of the a-form glycine crystal and the growth rate were studied. The aform glycine crystal is oriented in the high magnetic field in such a way that its crystallographic c-axis is at about 458 with the direction of magnetic field. This orientation is explained by the magnetic susceptibility anisotropy of the crystal stru...