This research work presents the results of an experimental investigation of cryogenically treated, coated and uncoated tungsten carbide cutting tool inserts in turning of AISI 1040 steel. Three different tungsten carbide inserts coated with aluminum chromium nitride (AlCrN), titanium nitride (TiN) and uncoated WC were taken and treated cryogenically. Experiments were performed to evaluate the c...

Metal-doped diamond-like carbon films were produced for the purpose of an electrochemical nanoelectrode. In this study we use Z-contrast scanning transmission electron microscopy to directly observe metal cluster formation and distributions within the chromium-doped carbon films. At low doping ~;6 at. % Cr!, Cr is uniformly distributed within the C matrix; at high doping ~;12 at. % Cr!, Cr-rich...

Allegheny Ludlum Type 316Ti (UNS S31635) is a titanium stabilized version of Type 316 molybdenum-bearing austenitic stainless steel. It is also known as DIN/EN designation No. 1.4571. The Type 316 alloys are more resistant to general corrosion and pitting/crevice corrosion than the conventional chromium-nickel austenitic stainless steels such as Type 304. They also offer higher creep, stress-ru...

In this study, the changes in microstructure of HP-Nb cast heat resistant steel after 8 years of service at high temperatures were investigated. Study of microstructure using optical microscopy (OM) and scanning electron microscopy (SEM) equipped with an energy dispersive spectrometry (EDS) showed that the microstructure of this steel in as-cast condition includes an austenitic matrix, and that...

A new pyrolysis technology involving chromium is proposed for the determination of δD in alkanes based on systematic analysis reaction temperature, conversion rate, and mechanism. Compared with traditional high-temperature (HTC) method, our findings suggest that chromium/high-temperature (Cr/HTC) can improve rate hydrocarbons reduce required temperature by up to 175 °C; meanwhile, increased an ...

Spark plasma sintering has been used for the first time to prepare the ASTM F75 cobalt-chromium-molybdenum (Co-Cr-Mo) orthopaedic alloy composition using nanopowders. In the preliminary work presented in this report, the effect of processing variables on the structural features of the alloy (phases present, grain size and microstructure) has been investigated. Specimens of greater than 99.5 per...

Composite powders of tungsten carbide with variable coating contents of Fe/Ni/Cr based alloys (1–15 wt.%) were prepared by sputtering. The coated powders have revealed a good performance to shape-forming and sintering. However, the presence of nanocrystalline coatings could enhance the formation of a brittle phase during sintering, named g-phase, (M,W)6C. To investigate this effect, the powders...

The microstructure, electronic structure and chemical bonding of chromium carbide thin films with different carbon contents have been investigated with high-resolution transmission electron microscopy, electron energy loss spectroscopy and soft x-ray absorption-emission spectroscopies. Most of the films can be described as amorphous nanocomposites with non-crystalline CrC(x) in an amorphous car...