Two significant advances are reported for solvent-based self-healing of epoxy materials. First, an autonomic system yielding complete recovery of fracture toughness after crack propagation was achieved by embeddingmicrocapsules containing amixture of epoxy monomer and solvent into an epoxy matrix. Healing with epoxy-solvent microcapsules is superior to capsules that contain solvent alone, and m...

In the present work, Na+-montmorillonite nanoclay (Na-MMT) was functionalized using 3-aminopropyltrimethoxysilane (3-APTMS) as a coupling agent. The covalent functionalization of MMT was confirmed by Fourier-transform infrared spectroscopy (FT-IR). In the specimen fabrication stage, 5 wt% of pristine MMT or silane-functionalized MMT (f-MMT) were incorporated into an epoxy system and the resulta...

The toughening of an aromatic amine-cured diglycidyl ether of bisphenoI-A epoxy with particles of crystalline polymers was studied. The crystalline polymers were poly(butylene terephthalate), nylon 6, and poly(vinylidene fluoride). Nylon 6 and poly(vinylidene fluoride) were found to toughen the epoxy about as well as did an equivalent amount of CTBN rubber. Poly(butylene terephthalate) was foun...

Vapor-grown carbon nanofibers (VGCNF) were functionalized with amine-containing pendants via a Friedel–Crafts acylation reaction with 4-(3-aminophenoxy)benzoic acid. The resulting H2N-VGCNF was treated with epichlorohydrin, followed by sodium hydroxide solution to afford N,N-diglycidyl-modified VGCNF that is designated as epoxy-VGCNF. Subsequently, epoxy-VGCNF was dispersed in an epoxy resin (E...

results the results showed that the epoxy plates 6 and 2 mm thick had the highest and the lowest averages of shielding effectiveness at 4.48 db and 1.90 db, respectively. however, increasing the thickness was useful up to 4 mm. in addition, in a similar attenuation pattern, x-band frequency was divided into lower, middle, and upper sections. the lower section had the highest shielding effective...

an epoxy resin was modified by silica nanoparticles and cured with an anhydride. the particles with different batches of 12, 20, and 40 nm sizes were each distributed into the epoxy resin ultrasonically. electron microscopy images showed that the silica particles were well dispersed throughout the resin. tensile test results showed that young’s modulus and tensile strength increased with the vo...

Epoxy – Polysulfide copolymers without or with low amounts of epoxy in their structure have poor mechanical properties in oxidative curing system.To strengthen the mechanical properties of polysulfide elastomer inclusion of epoxy resin (Epon828) as hard segment was studied. FT-IR spectroscopy and rheometry were used to verify the formation of epoxy-polysulfide copolymer.  Results obtained f...

In the printed circuit board assembly (PCBA) industry, integrated circuit (IC) dies are attached onto the printed circuit board (PCB) with epoxy. The die pads are first connected to the PCB tracks with gold or aluminium wires, utilising an ultrasonic wire-bonding machine. The dies are then coated with thermally cured epoxy. The chip-on-board (COB) is finally placed in an electrical oven for bak...

This paper investigated the effect of the amine-functionalized carbon nanotubes (CNTs) on the thermomechanical properties of CNT/epoxy nanocomposites. Mechanical stirring and ultra-sonication were utilized to uniformly disperse CNTs into the epoxy matrix. Non-functionalized and amine-functionalized CNTs with different weight percentages (wt. %) were mixed into the epoxy resin. Using standard te...