Solutions of histamine and methacholine bromide in different matrices for diagnostic purposes were analyzed for stability and quality control using capillary electrophoresis. Histamine (2,[4-imidazolyl]ethylamine) [CAS No. 51-45-6] was determined using a 0.1 M Tris-borate buffer of pH 8.3 with 5.10(-5) M cetyltrimethylammonium bromide (CTAB) and 0.005% poly(vinyl alcohol) (PVA) and detected at ...

Modified poly(aspartic acid)/poly(vinyl alcohol) interpenetrating polymer network (KPAsp/PVA IPN) hydrogel for drug controlled release was synthesized by a simple one-step method in aqueous system using poly(aspartic acid) grafting 3-aminopropyltriethoxysilane (KH-550) and poly(vinyl alcohol) (PVA) as materials. The hydrogel surface morphology and composition were characterized by Fourier trans...

Polyvinyl alcohol (PVA) nanocomposite films with sorghum starch nanocrystals (SSN) were prepared by incorporating various concentrations of SSN in PVA. SSN was isolated using acid hydrolysis of sorghum starch. The morphological studies of SSN using atomic force microscopy (AFM) revealed that the particle size varied from 65 nm to 68 nm. The mechanical properties of PVA-SSN nanocomposite films i...

A capillary electrophoresis tandem mass spectrometry (CE-MS/MS) method for the determination of four different sulfonamide antibiotics in commercial veterinary formulations has been developed. The samples were homogenized, solubilized in methanol, diluted in H2O/methanol (50:50, v/v), filtered, and injected, followed by electrophoretic separation in a polyvinyl alcohol (PVA)-coated capillary us...

depressive disorders are more common among persons with chronic diseases such as inflammatory bowel disease and anti-inflammatory effect of some antidepressants such as amitriptyline has been reported. acetic acid colitis was induced in both reserpinised (depressed) and non-reserpinised (normal) rats. reserpinised groups received reserpine (6 mg/kg, i.p.) one hour prior to colitis induction. th...

the acorn is an edible nut of oak trees (quercus spp.) that had been used for human nutrition for a long time. besides nutritious components, acorn contains considerable amounts of phenolic substances. at present study, two different varieties of iranian oak acorns, namely, q. branti var. persica (qb) and qcastaneifolia var. castaneifolia (qc) were used. the total polyphenol content measured in...

background & aim: clematis is an ornamental and medicinal plant that is primarily planted as an ornamental plant. clematis orientalis is native to asia and central europe, used as an antiseptic and refrigerant. the propagation of clematis is very important. in this study, the effects of plant growth regulators on rooting and growth of the plants in vitro culture were examined. experimental:...

introduction: otorrhea and granulation tissue in canal wall down mastoidectomy (cwd) is the common problem in cholesteatoma removal and leads to many discomfort for both the patient and the physician. the main objective in cwd is creating the dry cavity, so the topical antibiotic and acetic acid in variable saturations are used for this purpose. in this study we evaluate the effectiveness of to...