The paper deals with the application of X-ray fluorescence and diffraction for the routing control of a chemical content of an electrolysis cell in aluminum reduction plants. Among two approaches XRD meets technological requirements on accuracy, time limit and the cost of analysis. XRF demonstrates insufficient accuracy because of sample preparation problem.

.................................................................................................................................................................. 4 ZUSAMMENFASSUNG .............................................................................................................................................. 6 INTRODUCTION..............................................................

To determine the influence of electrochemical polarization of PtRu/C catalysts on methanol electrooxidation, this work investigated methanol electrooxidation on as received and different electrochemically polarized PtRu/C catalysts. Thermogravimetric analysis (TGA) and X-ray diffraction (XRD) were used to characterize the redox state of PtRu/C after different electrochemical polarization. The m...

Submit Manuscript | http://medcraveonline.com Abbreviations: ILs: Ionic Liquids; CMNPs: Citrate-Coated Magnetite Nanoparticles; TEOS: Tetraethoxyorthosilicate; CPTMS: 3-Cloropropyltrimethoxysilane; IM: Imidazole; XRD: X-Ray Diffraction; FT-IR: Fourier-Transform Infrared Spectroscopy; TGA: Thermal Gravimetric Analysis; VSM: Vibrating-Sample Magnetometer; SEM: Scanning Electron Microscope; TLC: T...

Activated carbon was treated at 5 GPa up to 1600 C, and the structural evolution in the graphitization process was investigated. The graphitization temperature is equal to 1200 C at 5 GPa, reflected by X-ray diffraction (XRD) patterns. Honeycomb-like structures in micron scale come into being in the high-pressure sintering temperature range of 100

Materials and methods: A total of 300 stones were obtained at Atatürk University, Faculty of Medicine Urology Clinic through open surgery, percutaneous nephrolithotomy (PNL), ureterorenoscopy (URS), and extracorporeal shock-wave lithotripsy (ESWL) between 1 January 2005 and 30 December 2008. Stones were analyzed in the laboratory of Ankara General Directorate of Mineral Research Exploration usi...

The co–polymer (Poly-ClBN) of 1, 2 Di-ChloroBenzene and Naphthalene has been synthesised. The copolymer (Poly-ClBN) has been characterised by X Ray Diffraction (XRD) and UV spectroscopic method. Thermo Gravimetric analysis (DTA, DTG and TG) has been used for analysis of thermal stability of the copolymer.

Cupric oxide (CuO) nanoparticles were prepared by the chemical route by calcinations at a higher temperature from 300 o C to 400 o C. For the comparison transmission electron microscopy (TEM) and x-ray diffraction (XRD) measurements were made through JCPDS. There is good agreement between data produced by spectroscopy and the microscopic measurements.

Nanoparticles of barium carbonate/oxalate have been synthesized in situ from barium nitrate and ammonium carbonate/oxalate by reverse micelle method. These particles were characterized using transmission electron microscope (TEM), fourier transform infrared (FTIR) and x-ray diffraction (XRD). The results indicate that rod-like barium carbonate (BaCO3) and spherical barium oxalate (BaC2O4) nanop...

in this research na-y was synthesized by hydrothermal method and used as support for preparation of sn/pt/na-y catalysts using two different tin precursors, bu3sn(cl) and sncl2.2h2o, by sequential impregnation, in which the pt  was deposited first and in the next step sn was deposited. the catalysts were characterized by h2 chemisorption, transmission electron microscopy (tem), scanning electro...