نتایج جستجو برای: x ray crystallography
تعداد نتایج: 669246 فیلتر نتایج به سال:
We demonstrate a high-brightness compact 9 keV electron-impact microfocus x-ray source based on a liquid-gallium-jet anode. A approximately 30 W, 50 kV electron gun is focused onto the approximately 20 ms, 30 mum diameter liquid-gallium-jet anode to produce an approximately 10 microm full width at half maximum x-ray spot. The peak spectral brightness is >2 x 10(10) photons(s mm(2) mrad(2)x0.1% ...
Structural biology has contributed tremendous knowledge to the understanding of life on the molecular scale. The Protein Data Bank, a depository of this structural knowledge, currently contains over 100,000 protein structures, with the majority stemming from X-ray crystallography. As the name might suggest, crystallography requires crystals. As detectors become more sensitive and X-ray sources ...
C20 of molecular structures for C70Br10 or C60Cl24, which have been later confirmed by X-ray crystallography (partially with the use of synchrotron radiation). For the mixture of two compounds with known X-ray structures, C60Cl28 and C60Cl30, the experimental IR spectra were interpreted by comparison with the calculated ones using subtle differences for compounds possessing very similar structu...
Charged-coupled device (CCD) detectors have been widely accepted as detectors for collecting X-ray diffraction images. The CCD detector offers a sensitive detection system well suited for diffraction analysis and, compared with other detectors on the market, a relatively rapid system for read-out of the collected image. The two predominant markets for the CCD detector have been those in which r...
High-resolution ribosome structures determined by X-ray crystallography have provided important insights into the mechanism of translation. Such studies have thus far relied on large ribosome crystals kept at cryogenic temperatures to reduce radiation damage. Here, the application of serial femtosecond X-ray crystallography (SFX) using an X-ray free-electron laser (XFEL) to obtain diffraction d...
Macromolecular Crystallography is expanding rapidly, with respect to the number of molecules studied and their significance to biology and medicine. This expansion is enabled by faster acquisition of high quality diffraction data, the development of efficient X-ray detectors and the expanded availability of high brilliance X-ray beam lines at synchrotron radiation facilities.
Phytochromes are a family of photoreceptors that control light responses of plants, fungi and bacteria. A sequence of structural changes, which is not yet fully understood, leads to activation of an output domain. Time-resolved serial femtosecond crystallography (SFX) can potentially shine light on these conformational changes. Here we report the room temperature crystal structure of the chromo...
The indexing methods currently used for serial femtosecond crystallography were originally developed for experiments in which crystals are rotated in the X-ray beam, providing significant three-dimensional information. On the other hand, shots from both X-ray free-electron lasers and serial synchrotron crystallography experiments are still images, in which the few three-dimensional data availab...
Strongly halogen-bonded complexes form between 4-alkoxyphenyl-4-pyridines and iodine as well the interhalogens ICl IBr. Examples are characterised by single crystal X-ray crystallography most show a liquid-crystalline SmA phase.
Multicluster molecules [Cp(*)IrS2C2(B10H10)]n(L)[n= 3 (L = tpt), 2 (L = bpy)], connected with pyridyl-based ligands, were prepared and characterized by X-ray crystallography.
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