1. Introduction One of the most important recent applications of sonochemistry has been to the synthesis and modification of inorganic materials [1-5]. In liquids irradiated with high intensity ultrasound, acoustic cavitation drives bubble collapse producing intense local heating, high pressures, and very short lifetimes; these transient, localized hot spots drive high energy chemical reactions...

The high mass transport caused by ultrasonic radiation in the preconcentration of trace metal species in anodic stripping voltammetry (ASV), leads to an order of magnitude enhancement in sensitivity. A Nafion-coated mercury thin-film working electrode is placed in a specially designed small-volume sonovoltammetric cell. The preparation and curing procedure for the Nafion film on a glassy carbon...

In the first and second stage nuclear program of Department of Atomic Energy (DAE), technologies are matured for Pressurised Heavy Water Reactors (PHWRs) and Sodium-Cooled Fast Breeder Reactors (FBRs). Pre-service-Inspection (PSI), In-Service-Inspection (ISI) and Post-Irradiation-Examination (PIE) procedures are carried out for mechanical components and structures/assemblies of these reactors, ...

The lethal effects of high-intensity airborne sonic (9.9 kc/sec) and ultrasonic waves (30.4 kc/sec) on spores of Bacillus subtilis var. niger ATCC 9372 were determined. The spores, which were deposited on filter-paper strips, were exposed to sound waves for periods varying from 1 to 8 hr, at a temperature of 40 C and a relative humidity of 40%. Significant reductions in the viable counts of spo...

NiMoO(4) nanorods have been successfully synthesized by sonochemical method process by using Ni(CH(3)COO)(2) · 4H(2)O and (NH(4))(6)Mo(7)O(24) · 4H(2)O as starting materials. Some parameters including ultrasonic power, ultrasonic irradiation time, stirring effect, solvent effect, and surfactant effect were investigated to reach optimum condition. The as synthesized nanostructures were character...

Nanoscale hydroxyapatite based ceramics are a relatively new form of materials that are currently being investigated for a number of potential biomedical applications. This study reports on a straightforward wet chemical method that uses calcium hydroxide and phosphoric acid as precursors. After chemical synthesis a conventional thermal treatment was used to produce an ultrafine hydroxyapatite ...

In the first and second stage nuclear program of Department of Atomic Energy (DAE), technologies are matured for Pressurised Heavy Water Reactors (PHWRs) and Sodium-Cooled Fast Breeder Reactors (FBRs). Pre-service-Inspection (PSI), In-Service-Inspection (ISI) and Post-Irradiation-Examination (PIE) procedures are carried out for mechanical components and structures/assemblies of these reactors, ...

Mechanical action can produce dramatic physical and mechanochemical effects when the energy is spatially or temporally concentrated. An important example of such phenomena in solids is the mechanical initiation of explosions, which has long been speculated to result from 'hot spot' generation at localized microstructures in the energetic material. Direct experimental evidence of such hot spots,...

Power Ultrasound During the sonication of liquids, the accoustic wavelength range between approx. 110 and 0.15 mm for frequencies of 18kHz and 10Mhz. This is significantly higher than those of molecular dimensions, resulting in that there is between the molecules and the accoustic field no direct coupling of chemical species. The effects of sonication are mostly generated by the ultrasonic cavi...

The classic method for measuring absorption coefficients ofmaterials requires adetermination of the temperature rise within a medium during ultrasonic irradiation. Serious errors may result from a viscous heating effect around the required thermocouple probe, and from heat lost by conduction to surrounding, cooler egions. A thermal pulse-decay technique is proposed and evaluated which allows fo...