نتایج جستجو برای: template removal
تعداد نتایج: 186024 فیلتر نتایج به سال:
Crack-free, anatase-based optical coatings with a refractive index down to 1.27, a porosity up to 80 vol%, and a tunable thickness up to 1.5 μm were fabricated. The extraordinary stability of the porosity upon thermally induced crystallisation and template removal was attributed to the combined effects of the presence of 10% molar silica in the inorganic phase, a flash treatment at 500 °C, and ...
Adsorption of methanol and ethanol over mesoporous siliceous material are studied in the current paper. The pure mesoporous silica is prepared using tetraethylorthosilicate (TEOS) as silica source and dodecylamine as template at low pH. The prepared material was characterized using nitrogen adsorption,nX-ray diffraction (XRD) and scanning electron microscopy (SEM). The adsorption kinetics of me...
For reconstruction of some craniofacial defects which may be caused by trauma, removal of cancer, or due to congenital absence, the procedure of bone grafting is necessary. In this paper we propose a method to identify an optimal donor site for autologous grafts. It is done by performing an optimization of appropriate surface based and voxel based similarity measures between donor region and a ...
The morphology of Pd nanostructures is a critical parameter for the control of Pd activity in these applications. Like other noble metals, the synthesis of Pd nanostructures with different morphologies has been a challenging task. Many attempts have been made to control the synthesis of Pd nanostructures using surfactants and polymers. However, the drawback of these approaches is the integratio...
Electrocardiographic (ECG) signals are emerging as a recent trend in the field of biometrics. In this paper, we propose a novel ECG biometric system that combines clustering and classification methodologies. Our approach is based on dominant-set clustering, and provides a framework for outlier removal and template selection. It enhances the typical workflows, by making them better suited to new...
A microparticle material of gold/polystyrene-coated hollow titania was successfully synthesized. The synthesis steps involved hydrothermal synthesis of a carbon sphere from sucrose as a template, coating of the carbon sphere with titania, removal of the carbon sphere to produce hollow titania, followed by coating of polystyrene on the surface of hollow titania and then attachment of gold nanopa...
Elaborate one-dimensional photonic crystals are constructed from a variety of organic and biopolymers, which can be dissolved or melted, by templating the solution-cast or injection-molded materials in porous silicon or porous silicon dioxide multilayer (rugate dielectric mirror) structures. After the removal of the template by chemical dissolution, the polymer castings replicate the photonic f...
A [2]rotaxane was produced through the assembly of a picolinaldehyde, an amine, and a bipyridine macrocycle around a Cu(I) template by imine bond formation in close-to-quantitative yield. An analogous [3]rotaxane is obtained in excellent yield by replacing the amine with a diamine, thus showing the suitability of the system for the construction of higher order interlocked structures. The rotaxa...
We demonstrate a new approach to synthesize several unique nanostructures by tuning the selective reactivities on individual symmetry-breaking segmented selenium nanorods (SBS-SeNRs). The segment-selective reactions from thiolated silane endowed the formation of float-like SBS-SeNR@SiO2 with a silica coating on the t-Se segment. Several other unique nanostructures were further synthesized by ap...
The Mobile IP (MIP) protocol for IP version 4 provides continuous Internet connectivity to mobile hosts. However, currently it has some drawbacks in the areas of survivability, performance, interoperability with protocols for providing QoS. We have proposed an alternative protocol, Mobile IP with Location Registers (MIP-LR), which overcomes some of these drawbacks and is closer to the “service ...
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