Odd electron diffraction patterns (EDPs) have been obtained by transmission electron microscopy (TEM) on silicon nanowires grown via the vapour-liquid-solid method and on silicon thin films deposited by electron beam evaporation. Many explanations have been given in the past, without consensus among the scientific community: size artifacts, twinning artifacts or, more widely accepted, the exist...

This review describes use of transmission electron microscopy (TEM) in wood and fiber analysis. Analytical techniques and sample preparation methods are used to localize substructures of the cell wall polymers and are discussed in this review. The ultrastructural features of the wood cell walls, the structures formed by microfibrils, and the distribution of cell wall polymers, as revealed by TE...

the perovskite-structured la2cuo4 nanoparticles (lco nps) have been synthesized via an ultrasonic-assisted co-precipitation route using octanoic acidas organic surfactant, and the phase composition, morphology, lattice parameters and size of nanoparticles  are characterized through fourier transform infrared spectroscopy (ft-ir), x-ray diffraction (xrd), scanning electron microscopy (sem) and t...

the aim of the present work was to prepare and characterize biopolymer nanocarriers and evaluate their suitability in possible oral delivery of insulin. the egg albumin biopolymer was used to prepare nanoparticles which were further characterized by fourier transformed infrared spectroscopy (ftir), transmission electron microscopy (tem), scanning electron microscopy (sem), zeta potential, dynam...

in this research na-y was synthesized by hydrothermal method and used as support for preparation of sn/pt/na-y catalysts using two different tin precursors, bu3sn(cl) and sncl2.2h2o, by sequential impregnation, in which the pt  was deposited first and in the next step sn was deposited. the catalysts were characterized by h2 chemisorption, transmission electron microscopy (tem), scanning electro...

a facile and simple method was proposed to control the size and shape of the mgo nano structures with high surface area in the presence of efficient and cheap templates like peg 200, peg 600, peg 4000 and sorbitol at low temperature within a little time. nano rods and nanoparticles have been achieved by applying these templates and altering other growth parameters. the products were characteriz...

cobalt chromite (cocr2o4) with normal spinel structure, shows catalytic activity for oxidation of unburned methane in the natural gas vehilcles (ngv). in this study, cocr2o4 nanoparticles were synthesized through a conventional co-precipitation technique and investigated for the catalytic combustion of methane. cobalt nitrate hexahydrate, chromium nitrate nonahydrate and ammonia solution (25%) ...

tm3+, yb3+ and tm3+/yb3+ doped lavo4 nanostructures were synthe-sized for the first time by using the hydrothermal method with the aid of la(ch3co2)3 as  lanthanum source in presence of oleic acid as surfactant. the products were characterized by x-ray diffraction (xrd), scanning electron microscopy (sem), transmission electron microscopy (tem), photoluminescence (pl) spectroscopy and uv–vis di...

electrosynthesis process has been used for preparation of zinc sulfide nanoparticles. zinc sulfide nanoparticles in different size and shapes were electrodeposited by electrolysis of zinc plate as anode in sodium sulfide solution. effects of several reaction variables, such as electrolysis voltage, sulfide ion concentration as reactant, stirring rate of electrolyte solution and temperature on p...

Amorphous Spherical Carbon with Nitrogen (SCN) active carbon has been prepared by carbonization of poly(vinylpyridine-divinylbenzene) (PVPDVB) copolymer. The PVPDVB dehydrogenation copolymer has been quantum chemically (QC) simulated using cluster and periodic models. Scanning electron microscopy (SEM), transmission electron microscopy (TEM) and energy dispersive X-ray (EDX) studies of the resu...