A method for determination of tricyclazole in water using solid phase extraction and high performance liquid chromatography (HPLC) with UV detection at 230 nm and a mobile phase of acetonitrile:water (20:80, v=v) was developed. A performance comparison between two types of solid phase sorbents, the C18 sorbent of Supelclean ENVI-18 cartridge and the styrene-divinyl benzene copolymer sorbent of ...

an investigation was made to study the residual activity and air- borne effect of pirimiphos- methyl, at 2g a.i./m2 in hut scale trials on different surfaces in kazeroun, and bandar-abbas, south of iran. in kazeroun area, bio-assay contact mortality test with pirimiphos methyl on mud, wood, cement and plaster surfaces, 54 days after hut spraying, decreased from 100% to 46.7%, 61.25%, 36.6% and ...

solid phase extraction (spe) cartridge embedded with octadecyl c18 chain bounded to silica particles were used for the isolation and trace enrichment of pesticides from water samples collected from cotton, rice growing and municipal areas. the eluents were analyzed with high performance liquid chromatography (hplc) using methanol (100%) as mobiles phase at different uv-visible wavelengths. ddt ...

A novel liquid chromatography-tandem mass spectrometry (LC-MS/MS) method was developed for trace residue determination of bicozamycin (BZM) in livestock products and seafoods. BZM was extracted from a sample with acetonitrile-water (4 : 1), followed by a two-stage SPE enrichment and cleanup. The first stage involved a styrene-divinylbenzene copolymer cartridge (GL-Pak PLS-2), and the second sta...

In order to determine phenolic compounds in water, we propose a method based on the reaction of phenolic compounds with 4-aminoantipyrine in the presence of peroxodisulfate at pH 10 to form antipyrine dye and the solid-phase extraction of dye with a Varian Bond Elut Plexa cartridge. Dye collected on the cartridge is eluted with acetonitrile and the absorbance is measured at 475 nm. In our exper...

A quick, simple and effective chromatographic method for the separation of beryllium from a wide range of elements is described. The elements selected comprise elements which can interfere with the determination of beryllium by inductively coupled plasma-atomic emission spectroscopy (ICP-AES) and elements which commonly occur in environmental and industrial sample matrices. Beryllium is separat...