The synthesis and characterization of a new series of mesogen-jacketed liquid crystal polymers, poly{2,5-bis[(para-substituted phenyl)oxycarbonyl]styrene}s, based on 2-vinylterephthalic acid are reported. These polymers formed very stable liquid crystal phases above the glass transition temperatures. A brief comparison of the properties of the new polymers with those of some previously reported...

n-propylsulfamic acid supported onto magnetic fe3o4 nanoparticles (mnps-psa) was investigated as an efficient and magnetically recoverable catalyst for the one-pot synthesis of substituted coumarins from the reaction of coumarin with variety aromatic aldehydes in high to excellent yield at room temperature under solvent-free conditions. the magnetic nanocatalyst can be readily recovered easily ...

reaction of dialkyl acetylenedicarboxylates 1a-c andpyrrole derivatives 2a-e in the presence of triphenylphosphite (tpp) was investigated and the effect of the pyrrole substitution was established. diastereoselectivity is observed with pyrroles, 2a,b, yieldingphosphonate ester derivatives 3a-f and 4,and their relative configuration is determined by 1h/13c and 31p nmr and confirmed by single x-r...

reaction of compound 1 with thiobenzarnide or substituted selenobenzamides afforded substituted pyrrolobenzothiazole or selenazoles (2) respectively. selenium dioxide oxidation of the semicarbazone 4 with selenium dioxide gave 6- benzenesulfonyl- 4,5-dihydro-pynolo [3,2-el benzoselenadiazole (5).

Altered tumour cell glycosylation in relation to cellular heterogeneity in human brain tumours remains relatively unexplored. It has been reported that meningiomas express variability in glycosylation properties; however only limited meningioma subtypes have been studied with lectins histochemistry. The aim of this study was to compare the binding pattern of biotinylated lectins in seven subtyp...

Neste trabalho, buscamos analisar os aspectos da correlação entre o uso tecnologia e a transformação digital na Indústria do Agronegócio, por meio de uma aplicação conceitual simples. Como exemplo, exploramos desenvolvimento estufa ambiente controlado, utilizando sensores atuadores para fornecer condições ideais ao cultura. Este trabalho foi desenvolvido como parte projeto P&D um convênio c...

Há uma crescente demanda por estudos que explorem a presença de mulheres na Engenharia fim compreender baixa representatividade deste grupo nesta área. Neste trabalho são apresentadas análises quantitativas sobre participação feminina no corpo discente dos cursos graduação em e Tecnologia da Universidade do Estado Amazonas (UEA). A coleta dados teve como base informações oficiais universidade p...