Porous Ti3SiC2 was fabricated with high purity, 99.4 vol %, through reactive sintering of titanium hydride (TiH2), silicon (Si) and graphite (C) elemental powders. The reaction procedures and the pore structure evolution during the sintering process were systematically studied by X-ray diffraction (XRD) and scanning electron microscope (SEM). Our results show that the formation of Ti3SiC2 from ...

The reoxidation rate of sponge iron pellets and briquettes and oxidation of pure iron powder with compressibility between 27% and 55% in air and within the temperature range 300-900°C has been investigated. Factors affecting the oxidation rate are presented. These include the effect of temperature, compressibility, and sintering of Fe-powder before and during the oxidation.

the purpose of this study was to investigate the deposition of the hydroxyapatite (ha) coating via the electrophoresis procedure. the ha deposition was performed in an ethanol, methanol, acetone and isopropanol suspension. methanol was found to be the best deposition media. among the different environmental conditions, including the encapsulation of the samples under two vacuum types of pressur...

Recent accreditation of titanium powder products for commercial aircraft applications marks a milestone in titanium powder metallurgy. Currently, powder metallurgical titanium production primarily relies on vacuum sintering. This work reported on the feasibility of powder sintering in a non-vacuum furnace and the tensile properties of the as-sintered Ti. Specifically, we investigated atmospheri...

ransparent polycrystalline alumina (PCA) is a promising replacement for sapphire. Its optical properties however are highly dependent on the rain size and residual porosity which need to be controlled for real inline transmittances (RIT), that are high enough for possible applications. To achieve high RITs, doping as well as pressure assisted sintering is often used. In this study spark plasma ...

In this work we give a detailed account of the use of small angle neutron scattering to study the properties of polymer mediated, self assembled nanoparticle arrays as a function of annealing temperature. The results from neutron scattering are compared with those obtained from x-ray diffraction. Both techniques show that particle size increases with annealing temperatures of 580°C and above. T...

Magnesium-substituted fluorapatite powders were synthesized by hydrothermal method, and their sintering behavior was investigated by dilatometry in the temperature range 25-1100°C. Analysis of the obtained powders by X-ray diffraction and (31)P NMR spectroscopy showed that the powders consisted of a single apatite phase and no amorphous phase has been formed. Compared to pure fluorapatite, the ...

This paper reported the uses of ark clam shell calcium precursor in order to form hydroxyapatite (HA) via the wet chemical precipitation method. The main objective of this research is to acquire better understanding regarding the effect of sintering temperature in the fabrication of HA. Throughout experiment, the ratio of Ca:P were constantly controlled, between 1.67 and 2.00. The formation of ...

This study examines the effects of different ZrB2 content on various mechanical properties and electrical conductivity of ZrB2/Y-TZP composite. Composites with ZrB2 content of up to 20 wt-% were particularly beneficial at the lower sintering temperature range by achieving greater densification and better hardness than Y-TZP monolith. In contrast to the trends estimated from rule of mixture, the...

The relationship between magnetic and mechanical properties has been studied as a function of composition, atmosphere and temperature for a series of MnZn ferrites. When processed in air, strength and permeability are critically dependent upon the formation of Md+ and ~ e ' + on sintering, and residual stresses introduced via subsequent (re)oxidation upon cooling. In Fe deficient femtes, proper...