Nano oxides of Manganese Nickel and Cobalt Nickel were synthesized by chemical coprecipitation method from the reaction of respective metal sulfides of manganese, nickel, cobalt and sodium carbonate using ethylene diamene tetra acetic acid as an effective capping agent. The carbonate precursors were heated at different temperatures so as to form their oxides. Through the X-ray line broadening t...

The present study investigates the significance of different coating process parameters on the corrosion behaviour of electrolessly deposited Ni-P-W coatings on mild steel substrate. The process parameters considered are concentration of nickel source, concentration of reducing agent, concentration of tungsten source and annealing temperature. The corrosion characteristic is evaluated by electr...

We have developed an automated data analysis method for atmospheric particles using scanning transmission X-ray microscopy coupled with near edge X-ray fine structure spectroscopy (STXM/NEXAFS). This method is applied to complex internally mixed submicrometer particles containing organic and inorganic material. Several algorithms were developed to exploit NEXAFS spectral features in the energy ...

In a group of families in northern Sweden, a mutation in the ENAM gene (predicted to produce a highly truncated protein) results in the local hypoplastic form of autosomal dominant amelogenesis imperfecta. In this study, sections of deciduous teeth from members of 3 of these families were examined by scanning electron microscopy (SEM) and the enamel mineral was analysed by energy dispersive X-r...

Dendritic Ag/Au bimetallic nanostructures have been synthesized via a galvanic replacement reaction (GRR) of Ag dendrites in a chlorauric acid (HAuCl4) solution. After short periods of time, one obtains structures with protruding flakes; these will mature into very porous structures with little Ag left over. The morphological, compositional, and crystal structural changes involved with reaction...

808 Ó WILEY-VCH Verlag GmbH, D-69469 Weinheim, 1998 0935-9648/98/1007-0808 $ 17.50+.50/0 Adv. Mater. 1998, 10, No. 10 1.504 Š). Patterns were indexed using TREOR or METRIC-LS programs. SEM/EDX was carried out on a JEOL JSM820 microscope, equipped with a Kevex Quantum Detector Delta 4, and a Hitachi SEM S-570. Infrared spectra were recorded on a Nicolet 205 spectrometer using KBr pressed discs. ...

Caffeine loaded magnetic nanoparticle was successfully synthesized and were characterized by Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X-ray analysis (EDX), thermo gravimetric analysis (TGA), differential thermal analysis (DTA) and vibrating sample magnetometer (VSM). The resulting nanocom...

Y-junction carbon nanotubes were synthesized by arc discharge method from composite anode made of graphite powder, coal tar and alloy catalysts consisting of Fe, Ni, Co and S element. The synthesis of Y-junction carbon nanotubes was carried out in a mixture gas of 200 Torr Ar and 100 Torr H2. The as-synthesized Y-junction carbon nanotubes were examined by scanning electron microscopy (SEM), tra...