Analysis of MCPD esters and glycidyl esters in vegetable oils using the indirect method proposed by the DGF gave inconsistent results when salting out conditions were varied. Subsequent investigation showed that the method was destroying and reforming MCPD during the analysis. An LC time of flight MS method was developed for direct analysis of both MCPD esters and glycidyl esters in vegetable o...

subsequent to phytochemical investigation on scutellaria lateriflora (labiatae) from mazandaran provincein iran, the wax ester fraction of the leaves has been investigated. using tlc, cc glc and glc-ms, the alkyl esters of the epicuticular wax was analysed. total concentration of the esters was 35% and it was shown to be composed of a homologous series having various chain lengths in the range ...

The liquefaction of crop residues in the presence of ethylene glycol, ethylene carbonate, or polyethylene glycol using sulfuric acid as a catalyst was studied. For all experiments, the liquefaction was conducted at 160°C and atmospheric pressure. The mass ratio of feedstock to liquefaction solvents used in all the experiments was 30:100. The results show that the acid catalyzed liquefaction pro...

The glycerolysis of methyl esters and triglycerides with crude glycerol. a coproduct from the transesterification of triglycerides, was studied. Three procedures were followed ior this conversion. The first procedure was a one-step glycerolysis with methyl esters. The second procedure was a two-step process. This proced~~re involved an initial partial glycerolysis with methyl esters, followed b...

Polyol concentrations were determined by selected-ion monitoring in 10 sample sets taken before dialysis and hourly for 4 h during dialysis. Predialysis concentrations (mumol/L) exceeding the upper limit of normal (mean + 2 SD; n = 33) were found for erythritol (25.4-59.0), threitol (11.5-46.7), and arabinitol (21.0-49.3) in all 10 cases; mannitol (2.7-62.0) in nine cases; and xylitol (0.7-1.3)...

an increase in the red cell's normal substrate, glucose, can produce changes in red cell metabolism.

We report the effect of a polyol-mediated annealing on nickel ferrite nanoparticles. By combining X-ray fluorescence spectroscopy, diffraction, and 57 Fe Mössbauer spectrometry, we showed that whereas as-prepared nanoparticles (NFO) are stoichiometric, annealed ones (a-NFO) not, since Ni 0 -based crystals precipitate. Nickel depletion from spinel lattice reduction in polyol solvent accompanied ...

Simple approaches to synthesize hybrid nanoparticles with magnetic and plasmonic functionalities, with high control of their shape and avoiding cytotoxic reactants, to target biomedical applications remain a huge challenge. Here, we report a facile, fast and bio-friendly microwave-assisted polyol route for the synthesis of a complex multi-material consisting of monodisperse gold nanotriangles a...