An alumina–zirconia composite containing 5 mol% zirconia was prepared by following a wet interaction process in aqueous medium via the sol–gel route. The formed hydrogel which was aged for proper growth and orientation at room temperature, was then dried at a low temperature to minimize agglomeration. The sol–gel derived precursor powder was properly characterized through determination of surfa...

Erosion corrosion of an usual carbon steel in a variety of aqueous slurries of 10% Al2O3 powder composed of 0.1M NaOH, concentrated cooling water (synthetic rather than natural), 3% NaCl, and 0.01M HCl was investigated from the electrochemical point of view. The total weight loss, Wt, was experimentally divided into the following three terms: the mechanical loss, Wm, the corrosion loss, Wc, and...

Controlling the size and shape of semiconducting nanocrystals advances nanoelectronics and photonics. Quantum-confined, inexpensive, solution-derived metal halide perovskites offer narrowband, color-pure emitters as integral parts of next-generation displays and optoelectronic devices. We use nanoporous silicon and alumina thin films as templates for the growth of perovskite nanocrystallites di...

Bioactive imidazole derivative absorbs in the UV region at 305 nm. The interaction of imidazole derivative with nanoparticulate WO3, Fe2O3, Fe3O4, CuO, ZrO2 and Al2O3 has been studied by UV-visible absorption, FT-IR and fluorescence spectroscopies. The imidazole derivative adsorbs strongly on the surfaces of nanosemiconductor, the apparent binding constants for the association between nanomater...

Production of nanostructured aluminum matrix composite powder by high energy ball milling is investigated. Scanning electron microscopy analysis as well as the tap and green density measurements were used to optimize the milling time needed for the completion of the mechanical milling process. Also, we studied the particles morphology and size distribution change with milling time and its corre...

The synthesis of nanocrystalline Fe3Al powder by mechanical alloying as well as the structural ordering of the synthesized Fe3Al particles during the subsequent thermal analysis were investigated. Mechanical alloying was performed up to 100 hours using a planetary ball mill apparatus with rotational speed of 300 rpm under argon atmosphere at ambient temperature. The synthesized powders were cha...

Nanocrystalline Ni1-xZnxFe2O4 (x = 0, 0.2, 0.3 and 0.4) mixed ferrite with cubic spinel structure was successfully prepared by the citrated sol-gel method followed by calcinations at 600 C. Characterization of the materials was performed by XRD. Indirect-heating sensors using as-prepared powders of mixed ferrite as sensitive materials were fabricated on an alumina tube with Au electrodes and Pl...

In this research, the high-energy planetary mill was employed to produce nanocrystalline Ti-50Al(γ)(at%) powders. Initial powders were mechanically alloyed in 99.9999% and 90% purities of Argon and also Air atmosphere with alloying times up to 50h. The effect of impurity of Argon atmosphere on the microstructure and the rate of phase transformation of Ti-50Al were investigated during mechanical...

Nanocrystalline magnesium hydride powder was synthesized by mechanical milling of MgH2 in a planetary ball mill for various times. The effect of MgH2 structure, i.e. crystallite size, lattice strain, particle size and specific surface area on the hydrogen desorption properties was investigated. A single peak of hydrogen desorption was observed for as-received powder, exhibiting an average parti...

We apply atomic force microscope for local electrostatic charging of oxygen-terminated nanocrystalline diamond (NCD) thin films deposited on silicon, to induce electrostatically driven self-assembly of colloidal alumina nanoparticles into micro-patterns. Considering possible capacitive, sp2 phase and spatial uniformity factors to charging, we employ films with sub-100 nm thickness and about 60%...