The preparation and characterization of metakaolin-based geopolymer mortars containing an organic epoxy resin are presented here for the first time. The specimens have been prepared by means of an innovative in situ co-reticulation process, in mild conditions, of commercial epoxy based organic resins and geopolymeric slurry. In this way, geopolymer based hybrid mortars characterized by a differ...

A fatigue test method by a miniaturized hourglass-shaped fatigue specimen has been developed for International Fusion Materials Irradiation Facility (IFMIF) and sufficient potential as the alternative to a conventional large specimen was presented. Furthermore, focused ion beam micro-sampling method was successfully applied to microstructural analysis on fracture process. Where, the effects of ...

Bicrystalline α-Fe2O3 nanoblades (NBs) synthesized by thermal oxidation of iron foils were reduced in vacuum, to study the effect of reduction treatment on microstructural changes and photocatalytic properties. After the vacuum reduction, most bicrystalline α-Fe2O3 NBs transform into single-layered NBs, which contain more defects such as oxygen vacancies, perfect dislocations and dense pores. B...

Certain microstructural features of materials, such as grain size in metals, porosity in ceramics, and structural phase compositions, are important for determining mechanical properties. Many of these microstructural features have been characterized by ultrasonic wave propagation measurements, such as wave velocity and attenuation. Real-time monitoring of ultrasonic wave propagation during the ...

Productions, mechanical and microstructural analyses of bioglass/sheep hydroxyapatite (SHA) composites are introduced. Bioglass were added to calcinated SHA with various concentrations 5 and 10 wt. %. Powder mixture compacted with pressure (350 MPa) in steel moulds to obtain cylinder samples. As the next step, samples sintered in air at various temperatures (1000, 1100, 1200, 1300 C for 4 hrs)....

Microstructural changes taking place during the heat treatment of cold-worked NiTi alloy are of key interest in shape memory alloy technology, since they are responsible for setting the austenite shape and functional properties of the heat-treated alloy. In this work, microstructural evolution during non-conventional electropulse heat treatment of thin NiTi filaments was investigated in a uniqu...