نتایج جستجو برای: mass spectroscopy

تعداد نتایج: 633953  

Journal: :international journal of bio-inorganic hybrid nanomaterials 0

2-[3-(2-formylnaphthoxy)-2-hydroxypropoxy] naphthaldehyde (1) have been prepared by reaction of 2-hydroxynaphthaldehyde with 1,3-dichloro-2-propanol. new n2o3 macro-acyclic ligands (l1, l2) synthesized from the reaction of (1) with aniline or cyclohexylamine. ni (ii), co (ii) and cu (ii) complexes was prepared from reaction of schiff-bases with metal chloride and nitrate salts. all of these com...

Journal: :Applied and environmental microbiology 1990
P F Ross P E Nelson J L Richard G D Osweiler L G Rice R D Plattner T M Wilson

Fumonisin B1 (FB1) and FB2 were isolated from corn cultures of both Fusarium moniliforme and Fusarium proliferatum. Respective concentrations in culture materials of FB1 and FB2 ranged from 960 to 2,350 and 120 to 320 micrograms/g for F. moniliforme and from 1,670 to 2,790 and 150 to 320 micrograms/g for F. proliferatum. Thin-layer chromatography, gas chromatography-mass spectroscopy, high-perf...

Journal: :Physical review letters 2015
D M Asner R F Bradley L de Viveiros P J Doe J L Fernandes M Fertl E C Finn J A Formaggio D Furse A M Jones J N Kofron B H LaRoque M Leber E L McBride M L Miller P Mohanmurthy B Monreal N S Oblath R G H Robertson L J Rosenberg G Rybka D Rysewyk M G Sternberg J R Tedeschi T Thümmler B A VanDevender N L Woods

It has been understood since 1897 that accelerating charges must emit electromagnetic radiation. Although first derived in 1904, cyclotron radiation from a single electron orbiting in a magnetic field has never been observed directly. We demonstrate single-electron detection in a novel radio-frequency spectrometer. The relativistic shift in the cyclotron frequency permits a precise electron ene...

2010
Hooi Ling Lee Issam Ahmed Mohammed Mohammed Belmahi Mohamed Badreddine Assouar Hervé Rinnert Marc Alnot

Two new mesogenic monomers, namely 3,3’-dimethoxy-4,4’di(hydroxyhexoxy)-N-benzylidene-o-Tolidine (Ia) and 4,4’-di(6-hydroxyhexoxy)-Nbenzylidene-o-Tolidine (IIa), were reacted with cadmium sulfide (CdS) via an in situ chemical precipitation method in ethanol to produce CdS nanocomposites. A series of different mass compositions of CdS with Ia and IIa ranging from 0.1:1.0 to 1.0:1.0 (w/w) were pr...

2002
L. PRATO M. SIMON T. MAZEH S. ZUCKER

Using high resolution near-infrared spectroscopy with the Keck telescope, we have detected the radial velocity signatures of the cool secondary components in four optically identified pre−main-sequence, single-lined spectroscopic binaries. All are weak-lined T Tauri stars with well-defined center of mass velocities. The mass ratio for one young binary, NTTS 160905−1859, is M2/M1 = 0.18±0.01, th...

2009
Mari Yamamoto Yukiyasu Kashiwagi Masami Nakamoto

A size-controlled synthesis of gold nanoparticles has been developed by the thermolysis of AuCl(SMe2) in the presence of alkylamines at 120 ◦C. In the procedure, the key intermediate was [Au(NH2R)2]Cl, detected by electrospray ionization (ESI) mass spectrometry. This thermally unstable intermediate was reduced by alkylamines under mild conditions to produce alkylamine-capped gold nanoparticles....

Journal: :Journal of synchrotron radiation 2012
Aleksandar R Milosavljević Christophe Nicolas Jean-Francois Gil Francis Canon Matthieu Réfrégiers Laurent Nahon Alexandre Giuliani

A novel experimental technique for tandem mass spectrometry and ion spectroscopy of electrosprayed ions using vacuum-ultraviolet (VUV) synchrotron radiation is presented. Photon activation of trapped precursor ions has been performed by coupling a commercial linear quadrupole ion trap (Thermo scientific LTQ XL), equipped with the electrosprayed ions source, to the DESIRS beamline at the SOLEIL ...

1995
J. J. Scherer R. J. Saykally

The cavity ringdown technique has been implemented for electronic spectroscopy of jet-cooled CuSi produced in a pulsed UV laser vaporization plasma reactor. A time-of-flight mass spectrometer is used to simultaneously monitor species produced in the supersonic expansion and allows correlation studies to be performed. Seven rotationally resolved vibronic bands have been measured near 400 nm, yie...

Journal: :The Journal of chemical physics 1996
J B Paul J J Scherer C P Collier R J Saykally

The cavity ringdown technique (CRLAS) has been employed to measure the gas phase absorption spectrum of the platinum silicide molecule in the 350 nm region. All nine of the measured rovibronic bands are assigned to a single 1 sigma-1 sigma electronic transition, with a ground state vibrational frequency of omega "e = 549.0(3) cm-1, and a bond length of r"0 = 2.069(1) angstroms. The results of...

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