نتایج جستجو برای: hollow fiber solidliquid phase microextraction
تعداد نتایج: 734692 فیلتر نتایج به سال:
a membrane bioreactor (mbr) system based on a dead-end immersed hollow fiber membrane and filamentous fungus aspergillus oryzae were used for treatment of baker’s yeast wastewater. the fungus was adapted to the wastewater in the bioreactor for two weeks before starting the continuous process. average organic loading rate of 4.2 kg cod/m3.d was entered the bioreactor. mbr system was able to redu...
The preparation and applicability of solid phase microextraction (SPME) fibers coated with a sol-gel organically modified silica based on 3-aminopropyltrimethoxysilane and polydimethylsiloxane (APTMS/PDMS) are described here. Micrographs of the coated fibers revealed a rugous surface; the thickness of the coating was estimated to be less than 30 microm. The APTMS/PDMS fibers were tested with sy...
Since solid-phase and liquid-phase microextraction (SPME and LPME) were introduced, as effective solvent-free methods, many efforts have been made to improve their modes and applications. However, due to limitations with sensitivity and efficiency, researchers have focused on improving the performance of their basic primary modes. In this way, in recent years, different methods such as ultrason...
We investigated the carrier-envelope phase (CEP) stability of hollow-fiber compression for high-energy few-cycle pulse generation. Saturation of the output pulse energy is observed at 0.6 mJ for a 260 μm inner-diameter, 1 m long fiber, statically filled with neon. The pressure is adjusted to achieve output spectra supporting sub-4-fs pulses. The maximum output pulse energy can be increased to 0...
In this paper, we have, for the first time, proposed an approach by combining self-assembled monolayers (SAMs) and nanomaterials (NMs) for the preparation of novel solid-phase microextraction (SPME) coatings. The self-assembly of octadecyltrimethoxysilane (OTMS) on the surface of ZnO nanorods (ZNRs) was selected as a model system to demonstrate the feasibility of this approach. The functionaliz...
This study developed an acid hydrolysis coupled to a solid-phase microextraction method employing a semi-microcolumn liquid chromatography system, instead of enzyme hydrolysis with solid-phase extraction for the pretreatment of human urine samples, to detect urinary 1-hydroxypyrene (1-OHP). The complete separation and detection of urinary 1-hydroxyprene was performed using a high-performance li...
A method for the determination of metolcarb and diethofencarb in apples and apple juice is developed using solid-phase microextraction (SPME) coupled with high-performance liquid chromatography (HPLC). The experimental conditions of SPME, such as the kind of extraction fiber, extraction time, stirring rate, pH of the extracting solution, and desorption conditions are optimized. The SPME is perf...
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