نتایج جستجو برای: hollow fiber solidliquid phase microextraction

تعداد نتایج: 734692  

Journal: :advances in environmental technology 0
mohammad j nosratpour isfahan university of technology morteza sadeghi isfahan university of technology keikhosro karimi isfahan university of technology saeid ghesmati isfahan university of technology

a membrane bioreactor (mbr) system based on a dead-end immersed hollow fiber membrane and filamentous fungus aspergillus oryzae were used for treatment of baker’s yeast wastewater. the fungus was adapted to the wastewater in the bioreactor for two weeks before starting the continuous process. average organic loading rate of 4.2 kg cod/m3.d was entered the bioreactor. mbr system was able to redu...

Journal: :Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 2008
André F P Biajoli Fabio Augusto

The preparation and applicability of solid phase microextraction (SPME) fibers coated with a sol-gel organically modified silica based on 3-aminopropyltrimethoxysilane and polydimethylsiloxane (APTMS/PDMS) are described here. Micrographs of the coated fibers revealed a rugous surface; the thickness of the coating was estimated to be less than 30 microm. The APTMS/PDMS fibers were tested with sy...

Since solid-phase and liquid-phase microextraction (SPME and LPME) were introduced, as effective solvent-free methods, many efforts have been made to improve their modes and applications. However, due to limitations with sensitivity and efficiency, researchers have focused on improving the performance of their basic primary modes. In this way, in recent years, different methods such as ultrason...

Journal: :Optics letters 2013
William A Okell Tobias Witting Davide Fabris Dane Austin Maïmouna Bocoum Felix Frank Aurélien Ricci Aurélie Jullien Daniel Walke Jonathan P Marangos Rodrigo Lopez-Martens John W G Tisch

We investigated the carrier-envelope phase (CEP) stability of hollow-fiber compression for high-energy few-cycle pulse generation. Saturation of the output pulse energy is observed at 0.6 mJ for a 260 μm inner-diameter, 1 m long fiber, statically filled with neon. The pressure is adjusted to achieve output spectra supporting sub-4-fs pulses. The maximum output pulse energy can be increased to 0...

Journal: :The Analyst 2012
Jingbin Zeng Haihong Liu Jinmei Chen Jianli Huang Jianfeng Yu Yiru Wang Xi Chen

In this paper, we have, for the first time, proposed an approach by combining self-assembled monolayers (SAMs) and nanomaterials (NMs) for the preparation of novel solid-phase microextraction (SPME) coatings. The self-assembly of octadecyltrimethoxysilane (OTMS) on the surface of ZnO nanorods (ZNRs) was selected as a model system to demonstrate the feasibility of this approach. The functionaliz...

Journal: :Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 2007
Hong-Wen Chen

This study developed an acid hydrolysis coupled to a solid-phase microextraction method employing a semi-microcolumn liquid chromatography system, instead of enzyme hydrolysis with solid-phase extraction for the pretreatment of human urine samples, to detect urinary 1-hydroxypyrene (1-OHP). The complete separation and detection of urinary 1-hydroxyprene was performed using a high-performance li...

Journal: :Journal of chromatographic science 2008
Xiu-Min Yang Ou Wang Ming-Zhao Wang Yan-Xue Hu Wei-Ning Li Zhi Wang

A method for the determination of metolcarb and diethofencarb in apples and apple juice is developed using solid-phase microextraction (SPME) coupled with high-performance liquid chromatography (HPLC). The experimental conditions of SPME, such as the kind of extraction fiber, extraction time, stirring rate, pH of the extracting solution, and desorption conditions are optimized. The SPME is perf...

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