BACKGROUND The effect of the extraction time (min) and temperature (°C) on the yield of betulinic acid (BA) from Zizyphus joazeiro barks using focused microwave-assisted extraction was investigated. MATERIALS AND METHODS The ethyl acetate was used as extractor solvent because it was shown to provide a betulinic acid-clean extract. A full two-level statistical factorial design was applied to d...

The aim of this study is to evaluate microwave-assisted extraction at several microwave power and time in extracting oil palm products, such as crude (CPO) fatty acid (PFA) composition. exposure was shortened overheating avoided when sterilized mesocarp exposed prior Soxhlet order obtain good quality oil. effects CPO PFA composition on the distillate produced were investigated. Gas chromatograp...

A sample preparation procedure using microwave energy is proposed for the determination of morphine, 6-acetylmorphine, codeine, cocaine, cocaethylene, benzoylecgonine, methadone, and 2-ethylene-1,5-dimethyl-3,3-diphenylpyrrolidine in human plasma. A screening asymmetrical factorial design was used to identify the most suitable extraction conditions as regards solvent, temperature, and extractio...

BACKGROUND The extraction of bioactive compounds from herbal materials requires optimization in order to recover the highest active dose. Response surface methodology was used to optimize variables affecting the microwave extraction of zerumbone from Zingiber zerumbet using the Box-Behnken design. The influence of variables, such as ethanol concentration (X1), microwave power (X2), irradiation ...

Hemp nut is commonly incorporated into several food preparations; however, most countries set regulations for hemp products according to their cannabinoid content. In this study, we have developed an efficient microwave-assisted extraction (MAE) method for cannabinoids (i.e., Δ9-tetrahydrocannabinol, cannabidiol, and cannabinol) in hemp nut. Optimization of the MAE procedure was conducted throu...

Microwave-assisted extraction of volatile oils (MAE) potentially offers a more efficient and bio-sustainable method than conventional extraction by Clevenger apparatus (CE). This study aimed to optimise the MAE of the volatile oil from Pterodon emarginatus fruits and characterise the volatile compounds. A 2³ full-factorial central composite design and response surface methodology were used to e...

In this paper, a microwave-assisted extraction (MAE) method was established for aristolochic acid-I from Aristolochiae Fructus, and the advantage of MAE was evaluated by chromatographic analysis coupled with nephrotoxicity studies. The experimental parameters of MAE for aristolochic acid-I in Aristolochiae Fructus were investigated and MAE was compared with Soxhlet extraction and ultrasound-ass...

Background and Objectives: Black mulberry is a juicy and dark purple to black fruit with a good balance of sweetness and tartness. This fruit is highly interested due to high quantities of anthocyanins. The bioactive compounds are often present in fruit tissues and should be released. The aim of this study was to extract bioactive compounds of black mulberries and assessment of heating process ...

This article performs an analysis of current limitations regarding the extraction of parallel behavioral models to reproduce the power amplifier (PA) nonlinear behavior and its dynamics. To overcome these limitations, a general preprocessing block that clearly improves the identification capabilities shown by classical parallel structures is proposed. It follows the principle of separating both...

Traditional hydrodistillation (HD), steam distillation extraction (SD), organic solvent extraction (SE), and microwave assisted hydrodistillation (MWHD) techniques were compared and evaluated for their effectiveness in the isolation of essential oil of Melissa officinalis from Algeria. The microwave assisted hydrodistillation technique was optimized in terms of both delivered power and time dur...