نتایج جستجو برای: facile synthesis
تعداد نتایج: 419180 فیلتر نتایج به سال:
organic solvents. In this study, NiFe2O4/sawdust nanocomposite was synthesized for removingoil pollutants. The oil-adsorbing nanocomposite could be easily separated from water bymagnet bar. The XRD results show tetragonal phase proving the composite formation. TheFESEM pictures successfully reveal the growth of NiFe2O4 on the sawdust template. The FTIRbands at 422 cm-1 and 615 cm-1correspond to...
CuAlS2 Chalcopyrite nanocrystalline are synthesized with facile method. The heat arrested solvothermal method for synthesize nanocrystalline were investigated. The time duration of synthesis, temperature of solution and metal salts to solvent molar ratio can be parameters that we are studied. The nanoparticles were synthesized with CuCl, AlCl3 and thiourea (SC(NH2)2...
A biotinylated heparosan hexasaccharide was synthesized using a one-pot multi-enzyme strategy, in situ activation and transfer of N-trifluoroacetylglucosamine (GlcNTFA) to a heparin backbone significantly improved the synthetic efficiency. The biotinylated hexasaccharide could serve as a flexible core to diversify its conversion into heparan sulfate isoforms with potential biological applicatio...
A facile procedure is described for the preparation of [14C]epicholesterol from [14C]cholesterol. Cholesterol is first converted to cholesteryl mesylate, which is treated with cesium acetate and 18-crown-6 in refluxing toluene to give epicholesteryl acetate. The latter is hydrolyzed, without isolation, with potassium hydroxide in tetrahydrofuran-methanol to give epicholesterol, which is obtaine...
A practical procedure for synthesizing cellulose nanospheres with sizes ranging from 60 to over 570 nm was developed. This methodology provides a near linear relationship between cellulose nanoparticle size and treatment time. The hydrolyzed nanocelluloses are predominantly cellulose II polymorphic crystalline structure and relatively uniform in particle size. 2007 Elsevier Ltd. All rights rese...
Graphene nanoribbons have attracted attention because of their novel electronic and spin transport properties, and also because nanoribbons less than 10 nm wide have a bandgap that can be used to make field-effect transistors. However, producing nanoribbons of very high quality, or in high volumes, remains a challenge. Here, we show that pristine few-layer nanoribbons can be produced by unzippi...
Here we report a simple procedure for generating colorimetric histone deacetylase (HDAC) substrates by solid-phase peptide synthesis based on racemization-free couplings of amino acid chlorides. We demonstrate the applicability of these substrates in HDAC assays.
Chitosan/multiwalled carbon nanotube nanocomposite has been successfully synthesized by the chemical method. The prepared nanocomposite was characterized using XRD, FTIR and HRTEM. The XRD pattern of the nanocomposite shows the presence of planes corresponding to both chitosan and MWCNT and the absence of impurity phases. The semi-crystalline nature of chitosan is also evident from the obtained...
BiCuOS, which is isostructural to the layered rare-earth oxysulfides LnCuOS (Ln = La-Eu), was synthesized by a single-step hydrothermal reaction at low temperature (250 degrees C) and pressure (<20 atm). Particular emphasis is placed on how the selection of the proper reaction conditions, such as temperature and pH, achieves a mutual high solubility of the metal-oxide reactants, Bi2O3 and Cu2O,...
Unorthodox chromophores enjoy the advantages of better hydrophilicity, large structural diversity, low-cost and facile synthesis, high chain flexibility good biocompatibility compared to conventional chromophores, leading many applications.
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