The possible relation between the properties of six commercial carbons and their gasification rates with carbon dioxide a t a series of temperatures between 900 and 1300” has been investigated. The following properties of the carbons have been determined: yantitative and qualitative ash analyses, hydrogen content, interlayer spacing, average crystallite size, true and apparent ensity, porosity,...

The influence of the addition of carbon on the crystalline structure and resistivity of polycrystalline silicon layers grown by simultaneous decomposition of SiH,, C^H. a n d P H T a t '°"° c w a s studied. Carbon content, morphology, preferred orientation, crystallite size, lattice strains and resistivity were determined. It was found that carbon has a pronounced effect on the crystalline stru...

Ba ferrite films with non-stoichiometric composition were deposited using Facing Targets Sputtering apparatus. The films with well c-axis orientation and remarkable perpendicular anisotropy were attained even at the substrate temperature below 600°C. Sufficiently large saturation magnetization 4 w o f 3.7 kGand small crystallite size below 20 nm were attained using the targets with Fe-excessive...

The morphological and microstructural changes during mechanical milling of Al powder mixed with 2.5, 5 and 10 wt.% Al2O3 particles were studied. The milling was performed in a planetary ball mill for various times up to 20 h. The produced composite powders were investigated using X-ray diffraction pattern (XRD) to elucidate the role of particle size, secondary phase content and milling time on ...

In this paper, three techniques to obtain capped magnetite nanoparticles were compared. In the formation of magnetite nanoparticles via the co-precipitation route, capping agents were introduced pre-, simultaneously with, or post-addition of the precipitating agent, ammonia. The amino acids L-glutamine and L-glutamic acid were used as the capping agents. Characterization via TEM, pXRD, EDX, and...

the nanostructured anatase tio2 with high thermal stability was prepared by polymeric sol-gel method without any additives. the particle size distribution of polymeric titania sol was determined by dynamic light scattering (dls). then properties of obtained titania were investigated by tg-dta, xrd, fesem and tem. also, the decolorization capability of resultant anatase was evaluated using methy...

in this investigation, hydroxyapatite (hap) nanostructure with uniform morphologies, controllable size, nano-dispersion and narrow-size distribution in diameter has been synthesized successfully by low-temperature hydrothermal process, and the as-synthesized powders were characterized by energy-dispersive x-ray spectroscopy, scanning electron microscopy, high-resolution transmission electron mi...

The determination of dislocation distribution parameters is discussed for specimens where both strain broadening caused by dislocations and size broadening occur. If the strain broadening is well described by a model due to Wilkens, several methods are possible for the analysis of the broadening of diffraction lines. In sputter deposited nickel layers, three different methods for diffraction li...

Many fractures occur in teeth that have been altered, for example restored or endodontically repaired. It is therefore essential to evaluate the structure and mechanical properties of these altered dentins. One such altered form of dentin is transparent (sometimes called sclerotic) dentin, which forms gradually with aging. The present study focuses on differences in the structure and mechanical...

Being endowed with an ability of capturing and releasing oxygen, the ceria surface conventionally assumes the role of catalyzing redox reactions in chemistry. This catalytic effect also makes possible its cytotoxicity toward microorganisms at room temperature. To study this cytotoxicity, we synthesized the doped and undoped ceria particles of 8-9 nm in size using an inexpensive precipitation me...