PURPOSE To present the findings from histological and chemical analysis of large dacryoliths and correlate them with previous reports. MATERIALS AND METHODS Dacryoliths were found in 8% of 216 dacryocystorhinostomy operations. In two cases with mild chronic dacryocystitis, large dacryoliths were extracted. The first case was a 42-year-old male with three dacryoliths in a lacrimal sac, present...

OBJECTIVE The aim of the present study was to determine the release of arsenic from 2 gray Portland cements, a white Portland cement, and 2 MTAs (ProRoot and MTA-Angelus). STUDY DESIGN The materials were manipulated and placed in plastic tubes, and the tubes were immersed in glass flasks containing water with grade reagent, pH 5.0. After 3 and 168 h, the water in which the material had been i...

A method for total calcium in serum was optimized, a dual double-beam atomic absorption spectrophotometer being used, with strontium as an internal reference. The effect of HCI and lanthanum concentrations on the signals of both calcium and strontium was determined. The final analysis was unaffected by known sources of interference in serum at a 50-fold dilution of serum in 50mmolar HCI contain...

A new, atomic absorption spectrophotometric method for serum iron and iron-binding capacity is described, which utilizes 20% (w/v) TCA plus heating at 90#{176} for 15 mm. This procedure liberates the ferric iron; precipitates the protein, facilitating removal by centrifugation; and avoids significant interferences by contaminating hemoglobin iron. The method is highly specific, accurate, and ha...

Ninetysix untreated patients with Malignant lymphoma's, 81 Hodgkin's disease and 15 Burkitt's lymphoma were studied for zinc (Zn) and selenium (Se) status. Plasma and hair Zn, and Se levels were measured by atomic absorption spectrophotometry. Chronic Zn and Se deficiencies (low plasma and low hair Zn and Se levels together) were found to be associated with Malignant lymphoma's in Turkish child...

We describe the rapid separation of inorganic arsenic plus metabolites from arsenobetaine or seafood arsenic in urine. Traditional, high-pressure liquid chromatography is replaced by disposable silica-based cation-exchange cartridges for this separation. Both fractions are quickly separated and collected for analysis by atomic absorption spectrophotometry. Analytical recovery of both fractions ...

Calibration in atomic-absorption spectrometry is achieved by means of a concentrationgradient chamber using a single concentrated standard solution. Calibration is rapid and extends over the entire working concentration range of the analyte, irrespective of the shape of the conventionally obtained calibration curve. No curve-fitting approximations are involved. With well-designed apparatus, dev...

We describe an integrated, molecular-absorbance, atomic absorption instrument for studying metal/ligand binding in clinical samples. For an interface between the "high-performance" liquid chromatograph and the atomic absorption instrument we used a flow-injection sample manipulator, thus allowing both the chromatograph and the atomic absorption detector to operate at their separate optimum cond...

For long-term pharmacokinetic studies in humans as well as in experimental animals, an analysis of strontium (Sr) with a low detection limit and high sensitivity is necessary. The data presented here describe the optimization of the furnace program and sample handling for measuring Sr in plasma by using graphite furnace atomic absorption spectrophotometry. The method was validated and applied t...