A program for quantitative evaluation of x-ray photoelectron spectra has been developed to serve as a practical tool for surface chemists. The program uses the ‘classic’ approach of quantification and requires as input the integrated intensities of the measured XPS lines. The usual correction methods and factors can be applied and controlled independently. All necessary basic data for calculati...

Photoelectron spectroscopy (PES) is one of the most established methods for determining the elemental composition and the chemical state of solid surfaces and thin films. This experiment focuses on X-ray Photoelectron Spectroscopy (XPS), which exploits Xray photons to excite electrons from the core levels of the atoms of a solid into the vacuum, thus probing the electronic structure of matter w...

The one-step synthesis and characterization of nanostructured metallic platinum microspheres by a low-pressure flat flame technique is presented here. Field emission scanning electron microscopy (FESEM), X-ray diffraction (XRD) and X-ray Photoelectron Spectroscopy (XPS) analyzed the as-derived powders. Collectively, the results obtained from these analyses confirmed the formation of microsphere...

X-Ray photoelectron spectroscopy (XPS) is a technique for identifying individual elements in a mixture/compound. Samples are irradiated by X-rays and the kinetic energy of ejected electrons is measured. Ejected electrons are captured by a spectrometer and measured intensities are plotted versus kinetic energy (Fig. 1). Each element appears as a series of peaks distributed as Gaussians/Lorentzia...

The purpose of this study is to develop an analytical method to quantify the nitrogen present at the surface of paper by using X-ray photoelectronic spectroscopy (XPS). A sample of softwood thermomechanical pulp (TMP) was treated with a cationic starch containing primary amines, while another one was treated with a cationic polymer containing quaternary amines. We also grafted monomers containi...

Free standing diamond thin films grown by the oxyracetylene frame method have been investigated by X-ray photoelectron spectroscopy (XPS) and Auger electron spectroscopy (AES). The radial distribution of the sp2-hybridized carbon species on the films and, consequently, the film quality, have been determined. While XPS does not seem to be an appropriate technique to distinguish between very smal...

background: motorcycle accidents and sport accidents lead yearly to many head injuries like head fractures and concussion. so finding the most proper helmet for reducing the injuries to head can be very helpful for head protection in such cases. methods: after 3d modeling of the helmet and head and meshing the model, a compressive impacting load of 1.31mpa was exerted on head and the model was ...

High pressure X-ray photoelectron spectroscopy (XPS) is used to characterize heterogeneous catalytic processes. The success of the new technique based on the possibility to correlate the catalytic activity and the electronic structure of an active surface. The dynamic character of a catalyst surface can be demonstrated impressively by this technique. In this contribution the basics of high pres...

This study investigated the effect of two different activation methods on the surface chemical composition of a CoCrMo-alloy. The activation was performed with oxygen plasma (OP) or nitric acid (NA). The surface physical-chemical properties were thoroughly characterized by means of several analytical techniques: X-ray photoelectron spectroscopy (XPS), time-of-flight secondary ion mass spectrome...