nano-cufe2o4 catalysts with different cu/fe molar ratios (cunfemo(n+1.5m)) were prepared by hydrothermal method. the thermal decomposition performance of cunfemo(n+1.5m) on cuso4 were determined with tg-dsc method to evaluate its catalytic activity and the roasted product was characterized by xrd. the results showed that cunfemo(n+1.5m) had superior catalytic properties and efficiency to cuso4 ...

a new tris-chelate cd(ii) complex, [cd(dadmbtz)3](clo3)2 has been successfully synthesized and characterized by ir, 1h, 13c nmr spectroscopy, elemental analysis and single crystal x-ray determination. the thermal behavior, uv-vis and fluorescence spectra of compound were studied. in reaction with dadmbtz, cadmium (ii) forms a tris-chelate complex with nearly c3 symmetry for coordination polyhed...

in this paper, cuo nanoparticles  have been synthesized via solid-state thermal decomposition using copper(ii) schiff base complexes as new precursors at 600ºc under air atmosphere for 3 h. surface morphology of the products were characterized by fourier transform infrared spectroscopy (ft-ir), x-ray diffraction (xrd) and scanning electron microscopy (sem).

in this study, we synthesis one-dimensional (1d) manganese(iii) schiff base coordination polymer [mn(brsalophen)(μ1,3-n3)]n by reaction of mncl2·6h2o and tetradentate schiff base ligand brsalophen at the presence of nan3 in methanol and characterized by elemental analyses (chn) and ft-ir spectroscopy. it was used as a new precursor to prepare spinel type manganese oxide nanowires by a facile so...

as a new precursor, [tris(2-hydroxyacetophenato) triaqua(iii)], [y(hap)3(h2o)3]; complex was used in thermal decomposition process for the synthesis of rod-like high-temperature ceramic ybco with length of about 320-350 nm and diameters 60–90 nm. the as-synthesized products were characterized by xrd, ft-ir, tem, sem and edx analyses. the results showed that by using fine raw materials, the calc...

The decomposition of lithium peroxide during the charging process of lithium-air batteries is investigated. A novel preparation method for electrodes in the discharged state, i.e., prefilled with Li2O2 using polyethylene oxide as a binder, is presented. The composition and reactivity of Li2O2-prefilled electrodes are examined by thermal analysis coupled with on-line mass spectrometry. Voltage p...