pure anatase titania (tio2), mixed 1.0 wt.% cerium-anatase titania (1.0 wt.%ceo2-tio2), and mixed 1.0 wt.% zirconia-anatase titania (1.0 wt.%zro2-tio2) nano powders were synthesized by co-precipitation method and characterized using x-ray diffraction (xrd), brunauer-emmett-teller (bet) surface area analysis, uv-vis diffuse reflectance spectroscopy (drs), and transmission electron microscope (te...

In this study, ITO nanoparticles (ITO-NPs) were reused from ITO target scraps to synthesize low cost ITO-NPs and to apply to make sputtering target for transparent conductive electrodes (TCEs). By controlling heat-treatment temperature as 980 °C, we achieved reused ITO-NPs having Brunauer, Emmett and Teller specific surface area (BET SSA) and average particle size 8.05 m2/g and 103.8 nm, respec...

The microwave-assisted synthesis of goethite nanoparticles has been studied. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), thermogravimetric analysis (TGA), differential thermal analysis (DTA) and Brunauer-Emmett-Teller (BET) method. Goethite rod-like nanoparticles have been successfully synthesized in 10 min of microwave treating at 100 °C. Part...

Monolithic macroporous zirconia (ZrO2) derived from ionic precursors has been successfully fabricated via the epoxide-mediated sol-gel route accompanied by phase separation in the presence of propylene oxide (PO) and poly(ethylene oxide) (PEO). The addition of PO used as an acid scavenger mediates the gelation, whereas PEO enhances the polymerization-induced phase separation. The appropriate ch...

Problems, which may arise when low-temperature nitrogen adsorption is used for the characterisation of porous materials, are discussed in this review. Continuous or discontinuous manometric techniques can be employed for nitrogen adsorption measurements at 77 K. For pore structure analysis, the nitrogen adsorption–desorption isotherms should be determined over the widest possible range of relat...

we report on the synthesis, morphology, chemically and structurally of la2o3-co3o4-zro2 nanostructure. the la2o3-co3o4-zro2 nanostructure was synthesized by a method based on the co-precipitation. composite powders have been characterized by xrd (x-ray diffraction), sem (scanning electron microscopy) and bet (brunauer-emmett-teller). x-ray diffraction showed the formation of nano crystalline, l...

the catalytic oxidation of toluene over copper oxide supported on natural diatomite was investigated. the catalyst was prepared by the wet impregnation method and characterized by using the brunauer emmett teller (bet), field emission scanning electron microscopy (fesem), x-ray diffraction (xrd), x-ray fluorescence (xrf) and temperature-programmed reduction (tpr) analysis. the highest catalytic ...

Silica nanoparticles were directly coated with cobalt hydroxide by homogeneous precipitation of slowly decomposing urea in cobalt nitrate solution. The cobalt hydroxide was amorphous, and its morphology was nanoflower-like. The BET (Brunauer-Emmett-Teller) surface area of the core-shell composite was 221 m²/g. Moreover, the possible formation procedure is proposed: the electropositive cobalt io...

Amino-functionalised metal-organic frameworks UiO-66 and -67 were post-synthetically modified with salicylaldehyde. A molybdenum complex was immobilised on the resulting materials. They were characterised by (13)C-MAS-NMR, XPS and PXRD to confirm immobilisation and stability. The immobilised complex is an active and reusable catalyst for olefin epoxidation with tert-butyl hydroperoxide (TBHP) a...

Hybrid organic aerogels consisting of polyvinyl alcohol (PVA), cellulose nanofibrils (CNFs), and graphene oxide nanosheets (GONSs) were prepared using an environmentally friendly freeze-drying process. The material properties of these fabricated aerogels were measured and analyzed using various characterization techniques including compression testing, scanning electron microscopy, thermogravim...