To find a suitable treatment in the preparation of Nb surface for platinum electrodeposition, different methods such as thermal oxidation, anodic oxidation, mechanical roughening, and mechanical roughening with subsequent anodic etching were examined. X-ray photoelectron spectroscopy was used to study the chemical composition of depth analysis of the surface. Moreover, in order to examine the m...

We show high resolution measurements of a surface plasmon resonance (SPR) sensor based on a rectangular nanohole array in a metal film. This SPR setup uses balanced intensity detection between two orthogonal polarizations of a He-Ne laser beam, which allows for sensitivity improvement, noise reduction and rejection of any uncorrelated variation in the intensity signal. A bulk sensitivity resolu...

the influence of mechanical polishing pre-treatments on steel substrates is investigated in terms of microstructure, deposition rate, adhesion, mechanical and corrosion properties of electroless Ni-P nanocoating with 9-10% wt. of P content. XRD analysis of Ni-P coatings demonstrated the nanocrystalline structure of coating with the grain size of 39 nm. Results showed that pretreatment of substr...

Oil-water emulsion flow behaviour was characterized with respect to surface chemistry. A state of the art stirred tank experimental set up was constructed that measured dynamic droplet size evolution with varying impeller speed. This technique was demonstrated with model Nexbase oil (with and without SPAN 80 surfactants) and water emulsions. Further, a CFD model for droplet size prediction was ...

The topic of this paper is optimized shading and lighting systems which consist of planar fins arranged along the edges of a quad-dominant base mesh, that mesh itself covering a reference surface. Such an arrangement can be observed e.g. in the Kogod courtyard roof designed by Foster + Partners for the National Portrait Gallery in Washington DC (Fig. 1): A reference surface consisting of three ...

preparation of 2-chlorobenzonitrile, and benzonitrile are reported here from the corresponding 2-chlorobenzaldehyde and benzaldehyde by the reaction of ammonium hydroxide/vpo titania, vpo bulk (ammonium metavanadate) cucr catalyst/air system in methanol. all these catalysts showed better conversions with reasonable selectivity to aromatic. the results prove that bet surface area results show vp...