نتایج جستجو برای: solvent free microwave extraction
تعداد نتایج: 758549 فیلتر نتایج به سال:
The use of rangeland medicinal plants and their active ingredients has recently been considered due to their therapeutic and industrial effects. In order to investigate the effect of height, plant limb, solvent and extraction method on some phytochemical properties of Verbascum speciosum in Chaharbagh rangelands, Golestan province, flower and leaf samples of this species were collected from alt...
Pomegranate seed oil was extracted in a closed-vessel high-pressure microwave system. The characteristics of the obtained oil, such as fatty acid composition, free fatty acidity, total phenolic content, antioxidant activity and colour, were compared to those of the oil obtained by cold solvent extraction. Response surface methodology was applied to optimise extraction conditions: power (176-300...
This research was undertaken to investigate the influence of extraction parameters during microwave-assisted extraction on total phenolic content, total flavonoids, total hydroxycinnamic acids and total flavonols of blackthorn flowers as well as to evaluate the antioxidant capacity by two different methods (2,2-diphenyl-1-picrylhydrazyl free radical scavenging capacity and ferric reducing antio...
a simple, fast, efficient and environmentally friendly method for synthesis of benzimidazole and its 2-alkyl, aryl and heteroaryl substituted derivatives was developed using zeolite hy. two component cyclolcondensation of 1,2-phenylenediamine (o-phenylenediamine) and commercially available carboxylic acids catalyzed by zeolite hy without any solvent, under microwave irradiation led to formation...
as benzimidazole ring is an important pharmacophore in modern drug discovery and benzimidazoles are very important intermediates in organic reactions, the preparation of benzimidazoles has gained considerable attention in recent years. here, a comparative study on the synthesis of benzimidazoles from aromatic, aliphatic and heterocyclic carboxylic acid, benzonitrile and o-phenylenediamine under...
A reliable and simple procedure to extract polychlorinated biphenyls (PCBs) from marine mussels using microwave energy is proposed. Freeze-dried mussels were subjected to MASE (Microwave Assisted Solvent Extraction) in a closed-vessel microwave system with n-pentane-sodium hydroxide (5 %) or dichloromethane-pentane (1:1) at different temperatures (70 and 90 oC), the extraction time was 10 minut...
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background & aim: a simple and rapid microwave- assisted extraction (mae) procedure was developed and optimized for the isolation of borneol and bornyl acetate from ferulago macrocarpa. ferulago macrocarpa (apiaceae) is an endemic plant in iran. experimental: dried powdered aerial parts of plants were soaked in water and irradiated with microwave in a clevenger extraction approach under opt...
Background and purpose: The use of rangeland medicinal plants and their active ingredients have recently been considered due to their therapeutic and industrial use. The quantity and quality of active ingredients in plants are influenced by environmental factors and ecological stresses of the area. One of the most important factors in extracting the active ingredients of plants is solvent, the ...
This article describes the various chemical components as obtained from the oils in the leaves of Cymbopogon citratus using hydrodistillation and solvent-free microwave extraction methods. Furthermore, extractions of the oils were also carried out with a slight in pH variation and compared, "GC-MS evaluation of C. citratus (DC) Stapf oil obtained using modified hydrodistillation and microwave e...
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