The residual stress field of HIPed Si3N4 rolling elements were studied. Two kinds of HIPed Si3N4 ball blanks self-finished at different nominal lapping loads ranging from 1.3kgf/ball to 10.87kgf/ball and four kinds of commercially finished 1⁄2′′ (12.7mm) HIPed Si3N4 balls before, during and after RCF tests were investigated. The experimental results showed that in the finishing process of HIPed...

Ni-Fe/Si3N4 nanocomposite coatings with various ratio of Si3N4 to Na-saccharine were prepared by electrodeposition technique. The effect of Si3N4 nanoparticulates in the Ni-Fe nanocomposite coatings was investigated in relation to the ratio of Si3N4 to Na-saccharine in the plating bath. X-ray diffraction analysis showed that the Ni-Fe nanocomposite coating has face center cubic structure (FCC)....

Textured silicon nitride (Si3N4) has been intensively studied over the past 15 years because of its use for achieving its superthermal and mechanical properties. In this review we present the fundamental aspects of the processing and anisotropic properties of textured Si3N4, with emphasis on the anisotropic and abnormal grain growth of β-Si3N4, texture structure and texture analysis, processing...

pH was used as the main driving parameter for specifically immobilizing silicon nanowires onto Si3N4 microsquares at the surface of a SiO2 substrate. Different pH values of the coating aqueous solution enabled to experimentally distribute nanowires between silicon nitride and silicon dioxide: at pH 3 nanowires were mainly anchored on Si3N4; they were evenly distributed between SiO2 and Si3N4 at...

This work deals with sintering additives for the low temperature pressureless sintering of Si3N4, via a transient liquid technique. Much attention has been given to the development of a sintering process using low-cost Si3N4 powder (Silzot HQ, Germany) as the starting material and employing sintering additives which are also both economically attractive and enable sintering at low temperatures....

The large-scale synthesis of Si3N4 nanobelts from quartz and graphite on a graphite-felt substrate was successfully achieved by catalyst-assisted carbothermal reduction-nitridation. The phase composition, morphology, and microstructure of Si3N4 nanobelts were investigated by X-ray diffraction, Fourier transform infrared spectroscopy, field-emission scanning electron microscopy, energy-dispersiv...

We have fabricated advanced metal–insulator–metal (MIM) capacitors with ultra-thin (200 Å) remote-PECVD Si3N4 dielectric layers having excellent electrical properties. The breakdown field strength of MIM capacitors with 200-Å-thick Si3N4 was larger than 3.5 MV/cm, which indicates the excellent quality of the deposited Si3N4 film. The main capacitance per unit area extracted by radio frequency (...

The chemical dry etching of silicon nitride (Si3N4)and silicon nitride (SiO2) in a downstream plasma reactor using CF4, O2, and N2 has been investigated. A comparison of the Si3N4 and SiO2 etch rates with that of polycrystalline silicon shows that the etch rates of Si3N4 and SiO2 are not limited by the amount of fluorine arriving on the surface only. Adding N2 in small amounts to a CF4 /O2 micr...

Using intermediate, liquid-forming compositions in the approach focuses on the Si3N4–R2O3 binary, where R2O3 is any (Y,La)2O3–AlN system as additives, fully dense Si3N4 ceramrare-earth oxide (or Y2O3) used singly or severally. After sinics with high strength at high temperature have been tering, this composition forms -Si3N4 and some refractory rareobtained by pressureless sintering. The cerami...

Excellent Fe3Si-Si3N4-SiC composites were successfully prepared with FeSi75 and SiC as main starting materials by nitridation reaction(at 1300°C for 8Hrs). The material properties were studied; the ferrosilicon nitridation mechanism was analyzed through chemical thermodynamics; phase composition, microstructure, corrosion resistance of products were also investigated. The results are shown that...