in this study a special type of silicoaluminophosphate with opal structure (opal-sapo) was prepared under microwave condition using tetraethylorthosilicate (teos), triethanolamine (tea), aluminiumisopropoxid and phosphoric acid 85%. the product was characterized by x-ray diffraction (xrd), thermogravimetric (tga) and fourier infrared spectroscopy (ftir).the crystalline product showed a good act...

Core-shell 12-tungstophosphoric acid/TiO2 (HPW/TiO2) nanoparticles at 10 and 20% of HPW have been synthesized by simple in-situ sol- gel method. Characterization of the samples was carried out by X-ray diffraction (XRD), Scanning electron microscopy (SEM), Fourier transform infrared (FTIR). The X-ray diffraction patterns of as prepared solid samples, indicated characterist...

Calcium fluoride nanoparticles with special amount of cerium ion (%1) were synthesized by coprecipitation. Fourier transforms infrared spectroscopy (FTIR), X-ray diffraction (XRD), absorption and photoluminescence (PL) from CaF2Ce nanoparticles has been investigated. FTIR spectra reveal that there are some amounts of OH, NO3 and other organic functional groups on the parti...

nanocrystals of zno were prepared by microwave irradiation using zn (ii) acetate and triethanol amin (tea) as the starting materials and water as solvent. the nanocrystals of zno with hexagonal (wurtzite) structure were characterized by x-ray powder diffraction (xrd), transmission electron microscopy (tem), scanning electron microscopy (sem), uv-vis absorption and ftir spectroscopy techniques.

the purpose of the current research is investigating the phenylalanine removal by using magnetic nanoparticles (fe3o4) from water samples. the effect of ph, contact time and phenylalanine concentration on phenylalanine adsorption efficiency by magnetite nanoparticles are studied in a batch system. transmission electron microscopy (tem), x-ray diffraction patterns (xrd) and fourier transform inf...

In this study, a polymer-silica nanocomposite using the sol-gel method was synthesized in three steps at room temperature. The nanocomposite material was formed with an organic compound (polyethylene glycol) and inorganic silica nanoparticles. Furthermore, the size and the distribution of nanoparticles in the polymer matrix were characterized by a transmission electron microscope (TEM).  In add...

an aqueous extract of pimpinella anisum was used for green synthesis of silver nanoparticles by bio reduction of an aqueous solution of silver nitrate. silver nanoparticles were characterized by uv–vis spectrometry, fourier transform infrared spectroscopy (ftir), x-ray diffraction (xrd) analysis, scanning electron microscopy (sem) and energy-dispersive x-ray analysis (edax). the increase in abs...

nano sio2/hyperbranched polyglycerol (hpg)/so3h catalyst was readily prepared for first time from inexpensive starting materials in aqueous media which catalyzed the synthesis of benzoic acid. ftir spectra, x-ray diffraction (xrd) and transmission electron micrographs (tem) was employed to characterize the properties of the synthesized nano sio2/hpg/so3h. high catalytic activity and ease of rec...

v2o5/sio2 nanoparticles was prepared via an one-pot sol gel method from vanadyl- acetylacetonate and tetraethylorthosilicate in refluxing meoh, followed by calcination at 700 °c for 2 hours. the resultant nanoparticles was characterized by means of scanning electron microscopy (sem), transmission electron microscopy (tem), x-ray diffraction (xrd), tga and ftir techniques. rapid and efficient ar...

the study describes the synthesis and characterization of zinc(ii) minoxidil nanocomposite (1). the reaction between zinc(ii) acetate, minoxidil, {c9h15n5o=minoxidil=(2,4-diamino-6-piperidine-1-yl) pyrimidine n-oxide)} as a ligand and ki as bridging agent, in methanol at 60°c leads to the formation of nano-sized zn(ii) minoxidil nanocomposite, 1. characterization of (1) was carried out by eleme...