نتایج جستجو برای: one pot solvent free synthesis

تعداد نتایج: 2797739  

Journal: :Catalysts 2023

An efficient and environmentally benign one-pot condensation of cyclic diketones, aldehydes naphthols was achieved with 1,4-diazabicyclo[2-2-2]octane supported on Amberlyst-15 as a novel catalyst, producing variety benzoxanthenones in good to excellent yields. The advantages this multicomponent reaction include the use heterogeneous solventless conditions simple methodology that is atom-economi...

Ahmad Shaabani, Ali Hossein Rezayan Rahim Ghadari

The synthesis of functionalized 2-oxo-2H-coumarin derivatives has been studied by a one-pot reaction of o-hydroxybenzaldehyde, ethyl 2-bromoacetate and triphenylphosphine in the presence of catalytic amount of triethyl amine in EtOAc, water or under solvent free conditions. We have found the best results obtained under solvent free condition.

Journal: :journal of sciences, islamic republic of iran 2015
s. kakaei h. sid kalal h. hoveidi

a simple and green chemical procedure was reported for the synthesis of dihydropyrimidinones from various aldehydes, ethyl acetoacetate and urea or thiourea using  holmium chloride as catalyst. the reactions were performed under solvent free conditions with ultrasound irradiation as the energy source. the advantages of this protocol include the excellent yield, operational simplicity, short tim...

Journal: :iranian journal of catalysis 2012
javad safaei-ghomi safura zahedi mohammad ali ghasemzadeh

an efficient green route for the preparation of naphthoxazinones, applying a three-component one-pot condensation reaction of 2-naphthol, aromatic aldehyde and urea in the presence of nano silica supported ferric chloride under solvent-free conditions has been developed. the present procedure offers several advantages such as short reaction time, simple workup, recovery and reusability of the c...

Journal: :organic chemistry research 0
farzaneh mohamadpour department of chemistry, faculty of science, university of sistan and baluchestan, p. o. box 98135-674 zahedan, iran malek taher maghsoodlu sistan & baluchestan university, zahedan, iran reza heydari department of chemistry, faculty of science, university of sistan and baluchestan, p. o. box 98135-674 zahedan, iran mojtaba lashkari department of chemistry, faculty of science, university of sistan and baluchestan, p. o. box 98135-674 zahedan, iran

an efficient and simple one-pot approach for the synthesis of 3,4-dihydropyrimidin-2-(1h)-one derivatives using antimony trichloride (sbcl3) as a mild catalyst by means of three-component biginelli reaction between β-keto esters, aldehyde derivatives and urea/thiourea under thermal and solvent-free conditions with excellent yields and short reaction times is reported. this methodology offers se...

Journal: :iranian journal of catalysis 0
mohammad ali ghasemzadeh department of chemistry, qom branch, islamic azad university, qom, p.o. box 364/37185. i.r. iran. zahra elyasi department of chemistry, qom branch, islamic azad university, qom, p.o. box 364/37185. i.r. iran.

this study introduces a green and efficient method for preparation of biologically-active substituted 4h-pyrans using the one-pot three-component reaction of aromatic aldehydes, dimedone and malononitrile in the presence of cobalt oxide nanoparticles. co3o4 nanoparticles were used as an efficient catalyst for the synthesis of polyhydroquinoline derivatives by the reaction of aromatic aldehydes,...

Journal: :iranian journal of catalysis 2015
leila dinparast hassan valizadeh

freshly prepared zno nanoparticles were used as an effective heterogeneous base catalyst for the synthesis of aryloximes. the conversion of arylaldehydes and arylketones into the corresponding oximes (up to quantitative yields) was achieved by simply mixing the liquid reactants and hydroxylamine hydrochloride with zno nanoparticles under solvent-free condition. the procedure was carried out und...

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