Ge and B diffusion was studied in nano-crystalline Si, and Pd and Si self-diffusion was studied in nano-crystalline Pd2Si during and after Pd/Si reactive diffusion. These experiments showed that grain boundary (GB) diffusion kinetic is the same in microand nano-GBs, whereas triple junction (TJ) diffusion is several orders of magnitude faster than GB diffusion. In addition, GB segregation and GB...

in this research zinc oxide (zno) nano-crystalline powders were prepared by sol-gel method using zinc acetate. the zno nanoparticles were characterized by x-ray diffraction (xrd), scanning electron microscopy (sem), ultraviolet-visible (uv-vis), fourier transform infra-red (ft-ir) and energy dispersive x-ray (edx) spectroscopy. the structure of nanoparticles was studied using xrd pattern. the c...

We have investigated the use of aluminum based amorphous metallic glass as the anode in lithium ion rechargeable batteries. Amorphous metallic glasses have no long-range ordered microstructure; the atoms are less closely packed compared to the crystalline alloys of the same compositions; they usually have higher ionic conductivity than crystalline materials, which make rapid lithium diffusion p...

Abstract There are various methods to produce iron based nano crystalline magnetic alloys. Among these methods, mechanical alloying is one of the most important. In this research, nano crystalline Fe85Si10Ni5 soft magnetic alloy was synthesized by mechanical alloying. The effect of alloying time on phase constituents and magnetic properties of the produced powders was investigated, by X-ray di...

hyperdiamonds are covalently bonded fullerenes in crystalline forms, more or less related todiamond, and having a significant amount of sp3 carbon atoms. design of severalhypothetical crystal networks was performed by using our original software programscvnet and nano-studio. the topology of the networks is described in terms of the netparameters and several counting polynomials, calculated by ...

In this communication we elucidate a microstructural picture of proton conduction in nano-crystalline yttria-stabilized zirconia at low temperatures (Kim et al. Adv. Mater., 2008, 20, 556). Based on careful analysis of electrical impedance spectra obtained from samples with grain sizes of approximately 13 and approximately 100 nm under both wet and dry atmospheres over a wide range of temperatu...

Synthesis of nano-crystalline alumina powder by a chemical pyrophoric reaction using citric acid and ammonia was investigated by varying the pH of the precursor solution, which played an important role in controlling the morphology of the synthesised powder. The flaky morphology obtained at pH = 2 could be modified to fine desegregated particulate form by varying the pH of the solution to 10. T...

the synthesis of nano- structured cobalt through a controlled chemical process followed by heat treating at various temperatures is studied. the product is characterized by icp, xrd, fesem , and tem, indicating that the as- synthesized particles have an amorphous structure with 1.76 for co/b ratio, an average size of 50 nm. the transformation of intermediate phases into single phase nano- cryst...

a organic-solution-processable functionalized-graphene (spfgraphene) material has been studied on pre-concentration and determination of trace mo(ii)ions. in this process, the effects of ph solution, elution conditions on pre-concentration of trace mo(ii) were studied and the effect of interfering ions was also investigated. a selective method for the fast determination of trace amounts of mo (...