A silver cluster having the composition Ag(9)(H(2)MSA)(7) (H(2)MSA = mercaptosuccinic acid) was synthesized in macroscopic quantities using a solid-state route. The clusters were purified by PAGE and characterized by UV-vis, FTIR, luminescence, and NMR spectroscopy, TEM, XPS, XRD, TG, SEM/EDAX, elemental analysis, and ESI MS. The solid-state route provides nearly pure Ag(9) clusters, and nanopa...

Single phase Eu doped GdMnO3 ceramics were prepared using solid state reaction route. Several different characterization techniques were used to investigate the structural and magnetic properties of the samples, including X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDX) and Vibrating Sample Magnetometer (VSM). All samples indicated single p...

In situ x-ray diffraction was used to optimize the synthesis of Aurivillius structure ceramic powders. Powders were prepared via conventional solid-state synthesis and the Pechini polymer precursor method. The phases Bi4Ti3O12, and Bi2Sr2Nb2TiO12 were studied. The Bi4Ti3O12 phase formed easily, regardless of processing route, between 400-500C and phase purity was achieved by 700C when using the...

the first aim of the present investigation was to prepare solid dispersions to improve the dissolution properties of oxcarbazepine and quetiapine using peg 6000 as a carrier with the help of two methods of preparations viz. spray drying and modified solvent method, and to compare the two methods. the second objective was to apply the modified solvent method for preparation of sustained release ...

this study aimed to evaluate enamel roughness after adhesive removal using different burs and an er:yag laser.the buccal surfaces of forty human premolars were sealed by two layers of nail varnish, except for a circular area of 3 mm in diameter on the middle third. the enamel surfaces were initially subjected to profilometry analysis and four parameters of surface irregularity (ra, rq, rt and r...