نتایج جستجو برای: microwaveassisted synthesis
تعداد نتایج: 409264 فیلتر نتایج به سال:
in this thesis, we exploit a simple and suitable method for immobilization of copper(ii) complex of 4?-phenyl-terpyridine on activated multi-walled carbon nanotubes [amwcnts-o-cu(ii)-phtpy]. this nanostructure was characterized by various physico-chemical techniques. to ensure the efficiency and fidelity of copper species, the implementation of three-component strategies in click-chemistry all...
in this thesis, a better reaction conditions for the synthesis of spirobarbiturates catalyzed by task-specific ionic liquid (2-hydroxy-n-(2-hydroxyethyl)-n,n-dimethylethanaminium formate), calcium hypochlorite ca(ocl)2 or n-bromosuccinimide (nbs) in the presence of water at room temperature by ultrasonic technique is provided. the design and synthesis of spirocycles is a challenging task becaus...
abstract in first part of this project, the use of a new and biguanid-like catalyst supported on silica as a recyclable catalyst provides a new route for the synthesis of a variety of arylalkylidene rhodanine derivatives through knoevenagle reaction in at present of solvent at room temperature. rhodanine derivatives and especially arylalkylidene rhodanines have proven to be attractive compound...
heteropoly acids (hpa) and their salts have advantages as catalysts which make them both economically and environmentally attractive, strong br?nsted acidity, exhibiting fast reversible multi-electron redox transformations under rather mild conditions, very high solubility in polar solvents, fairly high thermal stability in the solid states, and efficient oxidizing ability, so that they are imp...
this study investigated the impact of explicit instruction of morphemic analysis and synthesis on the vocabulary development of the students. the participants were 90 junior high school students divided into two experimental groups and one control group. morphological awareness techniques (analysis/synthesis) and conventional techniques were used to teach vocabulary in the experimental groups a...
The objective of the study was to optimize the processing of Microwave-Assisted Extraction (MAE) of flavonoids from Cryptotaenia japonica Hassk. The effects of processing parameters include ethanol proportion, extraction time, extraction temperature and ratio of liquid to solid on the flavonoids yield were determined and the optimal conditions for flavonoids were evaluated by means of Response ...
The oxodiperoxo complex MoO(O2)(2)(tbbpy) (tbbpy = 4,4'-di-tert-butyl-2,2'- bipyridine) was isolated from the reaction of MoO2Cl(2)(tbbpy) in water under microwaveassisted heating at 120 masculineC for 4 h. The structure of the oxodiperoxo complex was determined by single crystal X-ray diffraction. The Mo(VI) centre is seven-coordinated with a geometry which strongly resembles a highly distorte...
A sample preparation method based on the simultaneous microwaveassisted extraction–esterification (SMAEE) was developed for the determination of the fatty acid composition of foodstuffs by gas chromatography–mass spectrometry. The proposed sample preparation method was validated by comparison with the reference Soxhlet extraction method followed by derivatisation by ester formation and the same...
The carbon-carbon bond forming process is one of the most important transformations in organic synthesis aimed at the construction of complex molecules. In this regard, the Heck reaction poses as a pivotal synthetic methodology widely used for the formation of carbon-carbon bonds starting from olefins and an electrophile. An alternative of growing importance to the conventional Heck reaction wa...
یکی از مشکلات اساسی در rmmac کلاسیک این است که طراحی سیستماتیک این روش برای plant های ناپایدار امکان پذیر نمی باشد. مشکل اصلی در اینجاست که bpm برای plant های حلقه باز ناپایدار قابل محاسبه نیست. علاوه بر آن، تقسیم سیستماتیک زیرفضای نامعین در rmmac کلاسیک، وابسته به ابزار سنتز µ می باشد و دارای پیچیدگی های نسبتا زیادی است. برای حل مشکلات مذکور، در این تحقیق کنترل تطبیقی مقاوم به روش مدل چندگانه ...
نمودار تعداد نتایج جستجو در هر سال
با کلیک روی نمودار نتایج را به سال انتشار فیلتر کنید