نتایج جستجو برای: hydrothermal synthesis
تعداد نتایج: 422565 فیلتر نتایج به سال:
Miniaturized accelerometers are necessary for evaluating the performance of small devices, such as haptics, robotics and simulators. In this study, we fabricated miniaturized accelerometers using well-aligned ZnO nanowires. The layer of ZnO nanowires is used for active piezoelectric layer of the accelerometer, and copper was chosen as a head mass. Seedless and refresh hydrothermal synthesis met...
Recently, a cellulose-based composite material with a thin ZnO nanolayer-namely, ZnO nanocoated cellulose film (ZONCE)-was fabricated to increase its piezoelectric charge constant. However, the fabrication method has limitations to its application in mass production. In this paper, a hydrothermal synthesis method suitable for the mass production of ZONCE (HZONCE) is proposed. A simple hydrother...
Iron selenide obtained by mild hydrothermal reaction is not superconducting and exhibits a triclinic crystal structure below 60 K unlike superconducting FeSe from conventional solid state synthesis which is orthorhombic. In contrast, tetragonal iron sulphide FeS from hydrothermal synthesis is superconducting but undergoes no structural change on cooling.
Needle-like ZnO nanostructures were synthesized by an organic-free hydrothermal process. Thehydrothermal synthesis was performed at very low pressure (~20 kPa) with duration of process only 10min. The products were characterized by X-ray powder diffraction (XRD)and transmission electronmicroscopy (TEM).The XRD pattern indicated that the needle –like ZnO nanostructures were hexag...
Low-temperature aqueous chemical growth methods have shown great potential in the synthesis of ZnO nanostructures. Hexamethylenetetramine (HMTA) is the most common chemical substance used in the hydrothermal synthesis. In this study zinc oxide nanoparticles were prepared via hydrothermal growth using zinc acetate dihydrate and sodium hydroxide, as precursors instead of HMTA, as it is commercial...
Nano-sized BaTiO3 powders with particular Nb concentrations were prepared by Rotary- Hydrothermal (RH) method. Hydrothermal method was used at 180 °C for 5 hours with new Ti pressure and the teflon vessel was rotated at a speed of 160 rpm during the hydrothermal reaction. New hydrothermal method was used instead of previous solid state reaction for the system BaTiO3±Nb<sub...
Nano-sized BaTiO3 powders with particular Nb concentrations were prepared by Rotary- Hydrothermal (RH) method. Hydrothermal method was used at 180 °C for 5 hours with new Ti pressure and the teflon vessel was rotated at a speed of 160 rpm during the hydrothermal reaction. New hydrothermal method was used instead of previous solid state reaction for the system BaTiO3±Nb<sub...
Supercritical fluid (SCF) technology has become an important tool of materials processing in the lasttwo decades. Supercritical CO2 and H2O are extensively being used in the preparation of a great variety ofnanomaterials. The greatest requirement in the application of nanomaterials is its size and morphology control, which determine the application potential of the nanoparticles, as...
several samples of mesoporous silica were prepared via sol-gel chemistry in the presence of ctab as template with variation of stirring intensity and aging time, ratios of ctab/sio2 and nh4oh/h2o in synthesis mixture. effects of aging temperature, hydrothermal treatment and ter-butanol addition to the synthesis mixture on the textural properties of obtained samples were also studied. results of...
molecular sieves and zeolites are materials whose crystalline frameworks form nanometer or subnanometer pores. a variety of different crystal structures are known having a range of pore sizes. because the pore sizes are usually smaller than 2 nm, they are classified as microporous materials. synthesis of microporous materials is usually conducted by the high temperature treatment (80-200 °c) of...
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