A cation-excess (Ni,Mn) ferrite N~o.~zMno.51Fe2.0504.0 with a single phase was synthesized by heating the mixture of corresponding metal salts and oxide in 5% 02175% C02120% N2 gas mixture for 18h at 1100C. It could be thermochemically activated to form a cation-excess ferrite Nio,5z~l+s~Mno.51~l+6~Fe2~05~1+6~0440 in N2 gas at elevated temperature: The ( value was 0.03 1 at 1100C. The activated...

Magnetic nanoparticles of cobalt ferrite (CoFe204) have been synthesized using water-in-oil microemulsions consisting of water, cetyl trimethyl ammonium bromide (surfactant), n-butanol (cosurfactant), and n-octane (oil). Precursor hydroxides were precipitated in the aqueous cores of water-in-oil microemulsions and these were then separated and calcined to give the magnetic oxide. X-ray diffract...

Magnetic powder of Sr-ferrite was prepared by conventional and sol-gel auto-combustion methods. In conventional method, strontium carbonate and ferric oxide powders were mixed together and then mixture was calcined. In sol-gel auto-combustion method, a solution containing strontium nitrate, ferric nitrate and citric acid was heated until the combustion took place automatically; then, as-burnt p...

Bimagnetic monodisperse CoFe₂O₄/Fe₃O₄ core/shell nanoparticles have been prepared by solution evaporation route. To demonstrate preferential coating of iron oxide onto the surface of ferrite nanoparticles X-ray diffraction (XRD), High resolution transmission electron microscope (HR-TEM) and Raman spectroscopy have been performed. XRD analysis using Rietveld refinement technique confirms single ...

Oxide film properties and stress corrosion cracking (SCC) behaviour are investigated in the 308L stainless steel cladding layer with without being H-charged a deaerated high temperature water. Phase boundary (PB) has lower oxidation resistance than austenite ?-ferrite matrix. A compact Cr content-bearing inner oxide improves of phase H charging. H-induced PB penetration grain (GB) preferential ...

Monodisperse iron oxide nanocrystals were synthesized by a simplified method using iron chloride as precursor. In the presence of Cl ions, the as-produced iron oxide nanocrystals preferred a cubic shape with {100} facets exposed. The function of halogens including Cl and Br ions on stabilizing {100} facets of spinel structured iron oxides, rather than the regulation of thermolysis kinetics and ...

Mn-Zn ferrite cera~nics ~vere prepared tluoogh usual ceramic method osing d~tlkre~tt irou oxide ran malerials 'l'lic: micro-structure paran~eters. s11ch as the sinterm: density and the femite grain si/e. depended on hot11 tlic sintrrinf Iclnpcratirrc and the kinds of iron oxide raw materials. The differences in the niicrostrocture parametrr.: crc responsihlc I\)r v;~rialions ill nlagnetization,...

The properties of the oxide films grown on 308 L SS cladding with various surface treatments and temperatures in simulated PWR primary water are studied. thickness inner layer increases decrease roughness. high oxidation resistance ground is due to thicker fine-grained dislocations density subgrain boundaries near-surface. ferrite-affected zone (FAOZ) expands increase temperature, resulting fro...

The semiconductor spinel ferrite will have the chemical formula as AB2O4 (where A  divalent metal ion like Ni, Mn, Zn, etc and B  Iron metal ion Fe2 + and Fe3 +) and many studies have focused on the synthesis of nanomaterials because of extensive applications due to their novel properties. Magnetite and spinel ferrite nanocrystals are regarded as two of the most important inorganic nanomateri...