The formation of atoll garnet in the Ardara aureole, NW Ireland, is discussed using the textural, chemical and Electron Backscatter Diffraction (EBSD) data. Textural evidence suggests the possibility of incipient of garnet replacement from the core. In addition, the presence of staurolite and andalusite in the core of small atoll garnets as well as the occurrence of sillimanite in the core of l...

The present work gives a brief overview of the current status of the electron backscatter diffraction (EBSD) technique. The fundamentals of the production of Kikuchi patterns are first discussed. An experimental set-up for the automated obtaining and processing EBSD patterns in scanning electron microscopy (SEM) is subsequently described and the relevant calibration and automatic Kikuchi patter...

High operating temperatures can have very deleterious effects on the long-term performance of high-Cr, creep-resistant steels used, for example, in the structural components of power plants. For the popular creep-resistant steel X20CrMoV12.1 we analysed the processes of carbide growth using a variety of analytical techniques: transmission electron microscopy (TEM) and diffraction (TED), scannin...

Precession electron diffraction (PED) is a hollow cone non-stationary illumination technique for electron diffraction pattern collection under quasikinematical conditions (as in X-ray Diffraction), which enables “ab-initio” solving of crystalline structures of nanocrystals. The PED technique is recently used in TEM instruments of voltages 100 to 300 kV to turn them into true electron diffractom...

Two glasses of the compositions 2 BaO - TiO2 - 2.75 GeO2 and 2 BaO - TiO2 -3.67 GeO2 (also known as BTG55) are annealed at temperatures from 680 to 970 °C to induce surface crystallization. The resulting samples are analyzed by X-ray diffraction (XRD) and scanning electron microscopy (SEM) including electron backscatter diffraction (EBSD). Ge-Fresnoite (Ba2TiGe2O8, BTG) is observed at the immed...

The term “electron backscatter diffraction” (EBSD) is now synonymous with both the scanning electron microscope (SEM) technique and the accessory system that can be attached to an SEM. EBSD provides quantitative microstructural information about the crystallographic nature of metals, minerals, semiconductors, and ceramics—in fact most inorganic crystalline materials. It reveals grain size, grai...

Titania films have been grown on polycrystalline BaTiO3 (BTO) substrates at 7001C by pulsed laser deposition. Electron backscatter diffraction (EBSD) was used to determine grain orientations in the substrate before growth, and the phase and orientation of the supported films after growth. All BaTiO3 grains within 261 of (001) were covered by anatase films with an orientation relationship of (00...

A quantitative and automated phase analysis of dual-phase (DP) steel using electron backscatter diffraction (EBSD) was attempted. A ferrite-martensite DP microstructure was produced by intercritical annealing and quenching. An EBSD map of the microstructure was obtained and post-processed for phase discrimination. Band slope (BS), which was a measure of pattern quality, exhibited much stronger ...

The aim of this paper is to present the advantages of using Digital Image Correlation (DIC) and Infrared Thermography (IRT) to investigate the thermomechanical behavior of aluminum at the scale of its microstructure. The study combines these complementary imaging techniques: Electron Backscatter Diffraction (EBSD) to characterise the microstructure of the sample, DIC to obtain strain fields and...

the present study investigates the crystal preferred orientation (cpo) of quartz crystals in psammitic rocks to ascertain the deformationmechanism using electron backscatter diffraction (ebsd) on quartz crystals from north of the renvyle-bofin slide (rbs) nearletterfrack in western ireland. complete crystallographic orientations were determined for several thousand individual quartz crystalsin ...