The separation of a binary homogeneous azeotropic mixture using pressure swing distillation will be analysed on the example of acetonitrile/water. Two different processes are considered: the continuous heatand mass-integrated process and the inverted batch process. For both processes a model is developed and experimental data are given. In the paper the potential of the pressure swing distillat...

A shortcut procedure as quick, easy-to use method for design and simulation of multicomponent batch distillation is used to predict the operating condition of recovering xylene from solvent in an existing batch distillation column in benzol refinery. The procedure can be used to investigate the effect of the operating parameters on the operation of column for three possible modes of batch d...

One approach to active learning involves taking students through a guided exploration process; one which ensures students will observe phenomena and then be asked questions intended to draw conclusions regarding the observations. In recent years, this has been called inductive teaching, but more recently the expression “inquiry-based instruction” or related terms have become more common. Concur...

A new, general method for the determination of batch distillation regions of heteroazeotropic distillation is suggested. The method proposed, which means the extension of the method of Pham and Doherty, takes into consideration the possibility of the withdrawal of any fraction of either liquid phase from the decanter as distillate. The simplified and rigorous simulation calculations were carrie...

The multi®essel batch distillation column, as well as con®entional batch distillation, ( ) can be operated in a closed total reflux mode where the products are collected in ®essels along the column. A pre®iously proposed and simulated feedback control strategy for the closed operation is to indirectly adjust the ®essel holdups by using the reflux flow out of the ®essel to control the termperatu...

Multivessel batch distillation is a promising alternative to conventional batch distillation. Earlier studies proved the feasibility of temperature control in a closed operation mode, that is, when no product is removed until the end of the process. In this article, the influence of the reflux strategy during the initial start-up period is investigated in detail. This is a very important task i...

The separation of the homogeneous azeotropic mixture acetonitrile/water by pressure swing distillation (PSD) is considered. The PSD is operated as a discontinuous (batch) process and two batch modes, regular and inverted, are considered. The processes are analysed, aspects as to which batch mode should be preferred are discussed, and a dynamic model for both batch PSD processes is formulated. T...