The 3 rapid screening methods studied all involved chromatography of partially purified extracts on minicolumns. In one method acetonitrile-water is used to extract aflatoxin from corn and a lead acetate precipitation removes impurities from the extracts. The second method specifies acetone-water as the extracting solvent and ammonium sulfate as the precipitant. The third method is based on ace...

Mango leaf extract has proven to contain flavonoids that serve as antioxidants. In this study, a comparison between traditional maceration and sonication on flavonoid extraction from mango was investigated. The various ratios of ethanol acetone were utilized solvents (1:5, 1:10, 1:15). process, which uses an ultrasonic cleaning bath set at 40 oC, takes 30 minutes contrasted the procedure 36 hou...

Isopropyl has replaced ethyl alcohol in many such pharmaceutical preparations and cosmetics as mouth washes, dental solutions, and hair tonics. Although the physiology and toxicity of this material are fairly well known, a thorough knowledge of the metabolism involves a method for the separate determination of isopropyl alcohol and acetone, the chief product of its oxidation in the body. Many o...

Solvent-free Claisen-Schmidt reactions of cycloalkanones with various substituted benzaldehydes (aryl aldehydes) using solid NaOH (20 mol%) and applying a grinding technique were studied. Quantitative yields (96-98%) of α,α'-bis-(substituted-benzylidene)cycloalkanones were obtained. Aliphatic aldehydes also provided α,α'-bis-(substituted-alkylidene)cycloalkanones in very good yields with minor ...

in the present study, plumbago zeylanica linn. (plumbaginaceae) , one of the folk medicinal plants commonly used as antifertility agent was evaluated for its antifertility effect. five successive solvent extracts, petroleum ether, chloroform, acetone, ethanol and water extracts, of the stems of p. zeylanica were studied on estrous cycle at two dose levels, 200 and 400 mg/kg respectively.   of t...

It is demonstrated that solvent-saturated graphite oxide can be considered to be solid solvate, and two phases with distinctly different solvent composition are found near room temperature. Phase transitions between these two solvated phases were observed using synchrotron powder X-ray diffraction and DSC for methanol, ethanol, acetone, and dimethylformamide (DMF) solvents. Solvate A, formed at...

The aim of this study was to assess antioxidant properties of four in Lithuanian growing Nepeta varieties, namely N. cataria, N. cataria var. citriodora, N. transcaucasica and N. bulgaricum. The plants were extracted using different polarity solvents, namely acetone, methanol, ethanol and water. The antioxidant properties were assessed by determining total content of phenolics, using free DPPH•...

The aim of this study was to investigate the antioxidant activity of orange (Citrus auranthium) flesh (OF) and peel (OP) extracted with acetone, ethanol, and methanol. Antioxidant potential was examined by measuring total phenolic content (TPC), 2,2-diphenyl-1-picrylhydrazyl (DPPH) radical scavenging activity (RSA), total radical-trapping anti-oxidant potential (TRAP), oxygen radical absorbance...

In this study, we evaluated the suitability of six common organic solvents for gas chromatographic (GC) analysis of pesticides. Three of these, acetone, acetonitrile (MeCN) and ethyl acetate (EtAc), represent extraction solvents commonly used in multiresidue methods for determination of pesticides in produce. The other three, isooctane, hexane and toluene, often serve as exchange solvents befor...

We validated a canopy backscatter model for loblolly pine forest stands at the Duke Forest, North Carolina, by comparing the observed and modelled SAR backscatter from the stands. Given the SAR backscatter data calibration uncertainty, the model made good predictions of C-H H, C-HV, L-HH, L·HV, L-VV, P-HH, and P-HVbackscatter for most of 25 stands studied. The model overestimated C-VV backscatt...