Chlorinated organic solvents (COSs) are a significant threat to human beings. In this study, nanoscale bimetallic Ni/Fe particles were synthesized from the reaction of sodium borohydride (NaBH4) with reduction Ni2+ and Fe2+ in an aqueous solution. The zero-valent iron (nZVI) Ni-nZVI characterized by SEM (scanning electron microscopy), XRD (X-ray diffractometer), Brunauer–Emmett–Teller (BET), tr...