A solid bar microextraction (SBME) method containing sorbent materials 2 mg in the lumen of a porous hollow fiber membrane 2.5 cm for the extraction of carbamazepine, diclofenac and ibuprofen from river water samples is described. The desorbed analytes were analyzed using reversed-phase high performance liquid chromatography with ultraviolet detection. In order to achieve optimum performance, s...