نتایج جستجو برای: pxrd
تعداد نتایج: 684 فیلتر نتایج به سال:
Investigations of bacterial communities and characterization of mineralogy of the environment in the Złoty Stok As-Au deposit were carried out. PXRD analysis revealed the presence of picropharmacolite as the most common secondary arsenic mineral in the mine. Total DNA was extracted from slime streams or slime biofilms samples to investigate the bacterial communities. PCR amplification of 16S rD...
Desorption and subsequent rehydrogenation of Mg(BH4)2 with and without 5 mol % TiF3 and ScCl3 have been investigated. Temperature programmed desorption (TPD) experiments revealed a significant increase in the rate of desorption as well as the weight percentage of hydrogen released with additives upon heating to 300 °C. Stable Mg(BxHy)n intermediates were formed at 300 °C, whereas MgB2 was the m...
Three novel one-dimensional (1D) lanthanide coordination complexes involving the 4-methyl-3-nitrobenzoic acid (HL) ligand, with the general formulae [Gd(L)3(H2O)(CH3OH)] (1), [Gd(L)3(H2O)2]·(4,4'-bpy)·CH3OH (2), [Dy(L)3(H2O)(CH3OH)] (3), have been synthesized by solvothermal reactions. These complexes have been structurally characterized by single-crystal X-ray diffraction, IR, PXRD, TGA, and e...
Palm shell obtained from coastal part of southern India was studied for the removal for the adsorption of Hg (II) ions. Batch adsorption experiments were carried out as a function of pH, concentration of Hg (II) ions, time, temperature and adsorbent dose. Maximum removal was seen in the range pH 4.0pH 7.0. The palm shell powder used as adsorbent was characterized for its surface area, SEM, PXRD...
People may develop a headache, fatigue and even narcosis when the concentration of acetone in air is higher than 10,000 ppm. Hence, detecting and measuring acetone concentrations in the workplace or human body are necessary for our safety and health. Gas sensors play vital role in detecting, monitoring and controlling the presence of hazardous and poisonous gases in the atmosphere at very low c...
A novel three-dimensional two-fold interpenetrated bi-porous metal-organic framework IPM-325 (IPM: IISER Pune Materials) having pcu topology was synthesized at room temperature. Single crystal X-ray diffraction (SC-XRD) study revealed that the compound crystallizes in monoclinic lattice with molecular formula {[Zn(L)2 (SiF6)] (CH2Cl2) xG}n where G = Guests). All metal centers were found to have...
A unique hexagonal sheet-shaped NiO/CoO/Fe2O3 composite with irregularly shaped nanoparticles was fabricated for the first time through a simple co-precipitation and hydrothermal method. The NiO/CoO/Fe2O3 composite was characterized by numerous techniques (TEM, HRTEM, PXRD, EDX, ICP-AES, BET, and XPS) to confirm its structure and composition. This structure of the NiO/CoO/Fe2O3 composite may en...
The antibacterial and antibiofilm activity of chemically synthesized pure and Cu doped ZnO nanoparticles against marine biofilm forming bacteria has been reported for the first time. The synthesized nanoparticles were characterized using PXRD, FTIR and SEM which confirmed the formation of phase pure nanostructured zinc oxides. The antibacterial and antibiofilm activities of the synthesized nano...
The Crystallographic data of the α-DIPAB sample was measured using powder X-ray diffraction (PXRD). The crystal structure was also optimized using density functional based method. The calculations were performed both including van der Waals (vdW) interactions and excluding them to quantify the effects of vdW interaction on the crystal formation. The vibrational modes of DIPAB crystal correspond...
Macrocycle-to-framework strategy was explored to prepare covalent organic frameworks (COFs) using shape-persistent macrocycles as multitopic building blocks. We demonstrate well-ordered mesoporous 2D COFs (AEM–COF-1 and AEM–COF-2) can be constructed from tritopic arylene-ethynylene macrocycles, which determine the topology and modulate the porosity of the materials. According to PXRD analysis a...
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