Abstract In this present study, a novel method to fabricate bimetallic Fe-Co catalyst supported on waste silica was investigated for the photo-Fenton-like (PFL) degradation of Methylene Blue (MB) dye. The uniqueness work is preparation via fluidized-bed crystallization (FBC) process. Under optimum conditions initial pH 3.0, 3.0 mM H 2 O , and 1.0 g L -1 FBC-derived Fe-Co/SiO (fFCS), maximum res...