a novel, simple, sensitive and effective method has been developed for preconcentration of hg(ii) on nano-fe3o4-dop-ed solid-phase extraction adsorbent. in this paper, dioctyl phthalate (dop) was used to encapsulate nano-fe3o4 and produce a nano-fe3o4-dop sorbent based new sorbent was prepared. this was treated with ethylenediamine (ed) in another solvent-free procedure for the formation of a n...

An extraction-spectrophotometric method for cobalt determination in soils by the application of iodine nitrotetrazole chloride (INT) was developed and compared to atomic absorption spectrometry (AAS). The method investigated characterized with expressivity, selectivity and satisfactory accuracy.

BACKGROUND The aim of this paper was the validation of a new analytical method based on the high-resolution continuum source flame atomic absorption spectrometry for the fast-sequential determination of several hazardous/priority hazardous metals (Ag, Cd, Co, Cr, Cu, Ni, Pb and Zn) in soil after microwave assisted digestion in aqua regia. Determinations were performed on the ContrAA 300 (Analyt...

in present study we determine the zinc and lead levels in human blood samples by differential pulse polarography under optimum experimental conditions (ph=7.5, scan rate=5mv/s and pulse amplitude=50mv) the polarographic reduction peaks of zn and pb were examinedin the -0.72 v and-0.15 respectively. the zinc and lead content can be determined by in comparison with their standard solutions. accor...

Up until now there has been no direct method for detecting the electronic and magnetic structure of each atomic layer at the surface, which is an essential analysis technique for nanotechnology. For this purpose, we have developed a new method, diffraction spectroscopy, based on the photon energy dependence of the angular distribution of Auger electron emission. We have applied this method to a...

We have established and evaluated a flameless graphite cuvette method for copper in serum. This atomic absorption method provides substantial improvement in sensitivity, adequate accuracy, and acceptable precision, and little sample preparation is required before the analysis. Standard addition studies and measurements of National Bureau of Standards materials indicated that the proposed meth...

The capabilities and applicability of the radiotracer technique for methodological studies in hydride generation and electrothermal atomic absorption spectrometry are discussed and demonstrated by using several selected examples. It is shown that, for studying chemical and physico-chemical aspects of atomic absorption spectrometric methods, the radiotracer technique is superior to other techniq...