نتایج جستجو برای: intramolecular cyclization

تعداد نتایج: 18338  

Journal: :The Journal of biological chemistry 2007
Hisashi Takahashi Munehito Arai Tatsuyuki Takenawa Hiroyuki Sota Qui Hong Xie Masahiro Iwakura

Stabilization of an enzyme while maintaining its activity has been a major challenge in protein chemistry. Although it is difficult to simultaneously improve stability and activity of a protein by amino acid substitutions due to the activity-stability trade-off, backbone cyclization by connecting the N and C termini with a linker is promising as a general method of stabilizing a protein without...

2016
Maria Garrido Miriam Corredor Mar Orzáez Ignacio Alfonso Angel Messeguer

Apoptosis is a biological process important to several human diseases; it is strongly regulated through protein-protein interactions and complex formation. We previously reported the synthesis of apoptosis inhibitors bearing an exocyclic triazole amide isoster by using an Ugi four-component coupling reaction (Ugi-4CC), followed by a base-promoted intramolecular cyclization. Depending on the sub...

2010
Toshiaki Aoki Kensuke Ohnishi Masaaki Kimoto Satoshi Fujieda Kouji Kuramochi Toshifumi Takeuchi Atsuo Nakazaki Nobuo Watanabe Fumio Sugawara Takao Arai Susumu Kobayashi

We developed an efficient, stereoselective synthetic method for the diketopiperazine moiety of neoechinulin A and its derivatives. The intramolecular cyclization at 80 ºC proceeded with minimal racemization of the stereogenic center at C-12 on neoechinulin A, even though the cyclization at 110 ºC caused partial racemization. In contrast with these results, the cyclization on diketopiperazine of...

2018
Ancheng C. Huang Young J. Hong Andrew D. Bond Dean J. Tantillo Anne Osbourn

Sesterterpenoids are a relatively rare class of plant terpenes. Sesterterpene synthase (STS)-mediated cyclization of the linear C25 isoprenoid precursor geranylfarnesyl diphosphate (GFPP) defines sesterterpene scaffolds. So far only a very limited number of STSs have been characterized. The discovery of three new plant STSs is reported that produce a suite of sesterterpenes with unprecedented 6...

Journal: :Journal of the American Chemical Society 2007
Douglas C Beshore Amos B Smith

A full account of the enantioselective total syntheses of (+)-lyconadin A (1) and (-)-lyconadin B (2) is presented. Central to this venture was recognition and deployment of a key strategy-level intramolecular aldol/conjugate addition cascade that led, in a single operation, to two new carbon-carbon sigma-bonds, three new stereogenic centers, and two new rings, albeit with the incorrect stereog...

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