A novel, magnetic silica sorbent with polyelectrolyte multilayers (PEMs) on its surface was prepared, and was used for Magnetic Solid Phase Extraction (MSPE) of trace A+ via Flame Atomic Absorption Spectrometry (FAAS). The experimental parameters for the MSPE procedure, such as the pH, type, and concentration of eluent, ultrasonic time and effects of co-existing ions wer...

Background Correlation between metals may be useful in predicting toxicity to various biologically important organisms. The purpose of the current analysis was to evaluate the association of levels zinc, copper and iron in the ram blood serum, testicular tissue and epididymal tissue, and correlations of these elements to luteinizing hormone were investigated. MaterialsAndMethods Testis and bloo...

Brominated flame retardants (BFRs) are synthetic additives mainly used in electrical and electronic appliances and in construction materials. The properties of some BFRs are typical for persistent organic pollutants, and certain BFRs, in particular some polybrominated diphenyl ether (PBDE) congeners and hexabromocyclododecane (HBCD), are suspected to cause adverse health effects. Global consump...

amino acid profiling in routine clinical analysis (1,2). As analysts started using capillary electrophoresis (CE) in the 1990s, they were able to successfully use most of the popular reagents from LC analyses in electromigration techniques. The remarkable progress in detection technologies — such as diodearray ultraviolet (UV), laser-induced fluorescence, evaporative light-scattering, and mass ...

An improved derivatization protocol for the simultaneous determination of alkylphenol ethoxylates and brominated flame retardants with heptafluorobutyric anhydride under triethylamine amine base was investigated. The derivatization reaction was completed in 30 min at 50 °C using hexane as solvent. Under these conditions, it was observed that alkylphenol ethoxylates and tetrabromobisphenol A wer...

A new method for the determination of trace copper(II) in food samples by Cloud Point Extraction(CPE) combined with Flame Atomic Absorption Spectrometry(FAAS) is presented and evaluated. The method is based on the fact that hydrophobic complex of copper(II) with sodium diethyldithiocarbamate (DDTC) was formed at pH 6.0 and subsequently the hydrophobic complex was extracted into surfactant-r...

A method of video flame detection based on multi-feature fusion is presented in this paper. Physical characteristics of flame, including color clues, flame movement and flame flicker are incorporated into the scheme to detect fires in color video frames. Firstly, mean filtering was used to smooth the video frames and a flame color filtering algorithm was adopted to extract flame candidate regio...