نتایج جستجو برای: differential thermal analysis

تعداد نتایج: 3215083  

2017
Ali Kamal Attia Ahmed Sayed Saad Manal Sami Alaraki Eman Saad Elzanfaly

Purpose: Thermal analysis techniques have been applied to study the thermal behavior of fenbendazole (Fen) and rafoxanide (Raf). Semi-empirical molecular orbital calculations were used to confirm these results. Methods: Thermogravimetric analysis, derivative thermogravimetry, differential thermal analysis and differential scanning calorimetry were used to determine the thermal behavior and puri...

Journal: :Advanced pharmaceutical bulletin 2015
Ali Kamal Attia Eglal R Souaya Ethar A Soliman

PURPOSE Thermal analysis techniques have been used to study the thermal behavior of dapoxetine and vardenafil hydrochlorides and confirmed using semi-empirical molecular orbital calculations. METHODS Thermogravimetric analysis, derivative thermogravimetry, differential thermal analysis and differential scanning calorimetry were used to determine the thermal behavior and purity of the drugs un...

2006
E. C. Rodrigues A. B. Siqueira

Solid-state M-4-MeO-Bz compounds, where M stands for trivalent La, Ce, Pr, Nd and Sm and 4-MeO-Bz is 4-methoxybenzoate, have been synthesized. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy and complexometry were used to characterize and to study the thermal behaviour of these ...

2011
J. R. Locatelli C. T. Carvalho F. J. Caires M. Ionashiro

Solid-state Ln-L compounds, where Ln stands for heavy trivalent lanthanides (Tb-Lu) and L is malonate, have been synthesized. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy, TG-FTIR system, elemental analysis and complexometry were used to characterize and to study the thermal ...

Effect of nonlinear thermal radiation on the unsteady magnetohydrodynamic slip flow of Casson fluid between parallel disks in the presence of thermophoresis and Brownian motion effects are investigated numerically. A similarity transformation is employed to reduce the governing partial differential equations into ordinary differential equations. Further, Runge-Kutta and Newton’s methods are ado...

ژورنال: مواد پرانرژی 2014

In this study, the aging and deterioration mechanisms in the plastic bonded explosives (PBXs) and their components as well as standard methods for their evaluating are presented. Also, the techniques developed for the prediction of chemical lifetime and service life of PBXs will be reviewed and analyzed. These methods cite the lifetime prediction methods based on weight/energy loss by thermal a...

2009
W. B. Durham

Measurements of thermal conductivity and thermal diffusivity have been made on two samples of Climax Stock quartz monzonite at pressures between 3 and 50 MPa and temperatures between 300 and 523 K. Following those measurements, the apparatus was calibrated with respect to the thermal conductivity measurement using a reference standard of fused silica. Corrected thermal conductivity of the rock ...

2001
Xinwei Wang Hanping Hu Xianfan Xu

The photoacoustic (PA) technique is one of many techniques for measuring thermal conductivity of thin films. Compared with other techniques for thermal conductivity measurement, the photoacoustic method is relatively simple, yet is able to provide accurate thermal conductivity data for many types of thin films and bulk materials. In this work, the PA measurement in a high frequency range is mad...

A. Hassanzadeh Hassanzadeh H.G. Mohammadi R Khodabakhsh

The variation of thermal and structural properties of 2-{[4-(2-hydroxybenzylideneamino) phenylimino]methyl}phenol (PAM)Schiff base were studied using differential scanning calorimetry (DSC) and powder X-ray diffraction techniques before and after fast neutron (1.050 and 1.740kGy), beta (11.01Gy) and gamma (453.0Gy) irradiations. Under fast neutron irradiation, the melting and decomposition enth...

پایان نامه :وزارت علوم، تحقیقات و فناوری - دانشگاه صنعتی اصفهان - دانشکده شیمی 1389

in this thesis, a new optically active poly(amide-imide) (pai) was synthesized by the indirect polycondensation reaction of the l-phenylalanine based diacid chloride and 4,4?-diaminodiphenylether in the presence of triethylamine in n-methyl-2-pyrrolidone. the formation of pai was confirmed by ftir, 1h nmr and elemental analysis. in next step, the surface of titanium dioxide (tio2) nanoparticles...

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