نتایج جستجو برای: crystallite refinement
تعداد نتایج: 35490 فیلتر نتایج به سال:
the characterizations of natural diatomite from birjand deposit (iran) were studied such as chemical compositions, specific surface area, total pore volume, pore size distribution and xrd. the diatomite that was treated only with sulfuric acid displayed a larger surface area, expanded total pore volume and increased pore size in comparison with both washed natural diatomite with deionized water...
In this study the effect of crystallite size reduction and microstructure on the electrochemical corrosion behavior of nanocrystalline nickel (NC Ni) were investigated using Tafel polarization and electrochemical impedance spectroscopy (EIS) measurements in 10 wt.% NaOH. NC Ni coatings were produced by direct current electrodeposition using chloride baths in presence and absence of saccharin as...
SnO2 nanoparticles have been synthesized via sol-gel method in different annealing temperatures. TEM, FESEM and XRD techniques have been used to investigate the structure and morphology of SnO2 nanoparticles. The XRD pattern analysis shows all samples are single phase. XRD patterns show as the annealing temperature increases, the peaks become sharper which is related to the increase in the crys...
Diffraction line broadening analysis has been proved to be an extremely powerful method to study the defect properties of crystalline materials, since different types of defects produce different types of diffraction line profiles. In other word, the distribution of intensity, especially in tails of line profile, strongly depends on the crystallite size and dislocation structures. In this paper...
Recently, the Al2O3–TiO2–ZrO2 system has found valuable applications, particularly, as a support for NOx storage–reduction (NSR) catalysts. Nanocomposite powders were prepared from the co-precipitation method in inorganic precursors. The behaviors of mixed oxide nanoparticles under ultrasonic irradiation, such as dispersion, and crushing were studied. Phase transformations, crystallite size, an...
Graphite crystallizes in both hexagonal (2H) and rhombohedral (3R) systems. It is known that the 3R modification in graphite occurs locally by grinding of 2H crystal, and disappears by annealing at high temperature or decomposition of its intercalation compounds [Boehm 1955]. It was reported that the 3R phase content in artificial graphite, which was estimated from the integrated intensities of...
Yuri L. Zuev,1 Eliot D. Specht,1 Claudia Cantoni,1 David K. Christen,1 James R. Thompson,1,2 Rongying Jin,1 Athena S. Sefat,1 David G. Mandrus,1 Michael A. McGuire,1 and Brian C. Sales1 1Materials Science and Technology Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831, USA 2Department of Physics, University of Tennessee, Knoxville, Tennessee 37996-1200, USA Received 1 May 200...
We report strong magnetism in pure carbon films grown by electron irradiation assisted physical vapor deposition in electron cyclotron resonance plasma. The development of graphene nanocrystallites in the amorphous film matrix, and the dependence of the magnetic behavior on amorphous, nanocrystallite and graphite-like structures were investigated. Results were that the amorphous structure shows...
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